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  • Molecular Diversity Preservation International  (464)
  • Wiley-Blackwell  (126)
  • 2020-2022  (229)
  • 2015-2019  (234)
  • 1995-1999  (127)
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Keywords
Publisher
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  • 1
    Electronic Resource
    Electronic Resource
    Equilibria Between Gas and Liquid Phases for Concentrated Aqueous Solutions of Nitric Acid (1999)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 1999 (1999), S. 277-285 
    Details
    ISSN: 1434-1948
    Keywords: Nitric acid ; Nitrogen oxides ; Electrochemistry ; Thermodynamics ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Calculated diagrams, representing chemical and electrochemical properties of concentrated aqueous nitric acid mixtures, have been drawn for temperatures of 25 °C and 100 °C using vapor pressures and thermochemical data of related gaseous species. Electrochemical measurements have permitted the establishment of an experimental potential scale (referenced to the saturated mercurous sulfate electrode at 25 °C) incorporated in the diagram at 100 °C. These measurements also allowed the determination of the Gibbs free energy of formation of dissolved nitrous acid for various nitric acid solutions at 100 °C, leading to a value of ΔGf(HNO2) = -36.31 kJ mol-1, for the whole nitric acid concentration range.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    On the Optical Diagnosis and Sizing of Spherical Coated and Multilayered Particles with phase-Doppler anemometry (1996)
    Weinheim : Wiley-Blackwell
    Particle and Particle Systems Characterization 13 (1996), S. 104-111 
    Details
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: After having recalled basic theoretical results concerning the extension of generalized Lorenz-Mie theory to the case of multilayered spheres, results connected with phase-Doppler anemometry are considered, showing the influence of Gaussian beam intensity profiles on the light scattering properties of these particles. Particular emphasis is placed on the case of water-coated carbon core particles, for which the possibility of obtaining simultaneous size measurements of the core and outer diameters is discussed. The sensitivity of the technique to particles with a refractive index profile is also considered, showing that this technique is more sensitive to changes in the average refractive index of the particles than to refractive index profiles, such as produced by high pressure and temperature stresses, at least for the studied geometry.
    Additional Material: 10 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/ppsc.19960130208
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  • 3
    Electronic Resource
    Electronic Resource
    Phase-Doppler Anemometry with the Dual Burst Technique for measurement of refractive index and absorption coefficient simultaneously with size and velocity (1996)
    Weinheim : Wiley-Blackwell
    Particle and Particle Systems Characterization 13 (1996), S. 112-124 
    Details
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: The principle of the dual burst technique (DBT) based on phase-Doppler anemometry (PDA) is proposed for simultaneous particle refractive index, size and velocity measurements. This technique used the trajectory effects in PDA systems to separate the two contributions of the different scattering processes. In the case of forward scattering and refracting particles, it is shown that from the phase of the reflected contribution, the particle diameter can be deduced, whereas from the refracted contribution the particle refractive index and velocity can be obtained. Furthermore, the intensity ratio of these two scattering processes can be used for absorption measurements. Simulations based on generalized Lorenz-Mie theory and experimental tests using monodispersed droplets of different refractive indices and absorption coefficients have validated this technique.
    Additional Material: 19 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/ppsc.19960130209
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  • 4
    Electronic Resource
    Electronic Resource
    Simultaneous kinetic and microdielectric studies of some epoxy-amine systems (1998)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part B: Polymer Physics 36 (1998), S. 2911-2921 
    Details
    ISSN: 0887-6266
    Keywords: epoxy ; amine ; microdielectrometry ; conductivity ; conversion ; glass transition temperature ; curing ; Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Three reactive epoxy-amine systems based on diglycidyl ether of bisphenol A (DGEBA) with 4,4′-diaminodiphenylsulfone (DDS), 4,4′-methylenebis [3-chloro 2,6-diethylaniline] (MCDEA), and 4,4′-methylenebis [2,6-diethylaniline] (MDEA), were studied during isothermal curings at 140 and 160°C. The simultaneous kinetic and dielectric studies allow to express conductivity, σ, in terms of conversion, x, and of glass transition temperature, Tg. The conductivity, σ0, of the initial monomer mixture and, σ∞ of the fully cured network are measured. It is found that: The glass transition temperature, Tg, versus conversion, x, curves follows the equation of Di Benedetto modified by Pascault and WilliamsThere exists a linear relation between log σ/log σ0 and Tg.So, it is possible to predict both kinetic and dielectric behaviors of these epoxy-amine systems by the knowledge of Tg0, ΔCp0, and σ0, respectively, glass transition temperature, heat capacity, and conductivity of initial monomer mixture, Tg∞ and ΔCp∞, and σ∞, respectively, glass transition temperature and heat capacity and conductivity of fully cured network. © 1998 John Wiley & Sons, Inc. J Polym Sci B: Polym Phys 36: 2911-2921, 1998
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
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  • 5
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    Externally Heated Hollow Cathode Arc Plasma Source for Experiments in Plasma Wakefield Acceleration (2019)
    Molecular Diversity Preservation International
    Details
    Publication Date: 2019-09-10
    Description: An externally heated, hollow cathode arc source was recommissioned at UCLA for use in experiments to drive plasma wakefields with shaped beams at the Argonne Wakefield Accelerator. The hollow cathode arc source provides a robust plasma column with a density in the 10 13 – 10 14 cm − 3 range while external heating of the cathode allows the plasma arc regime to be accessed with applied voltages down to 20 V. Overall source operating principals are described, along with time-resolved plasma current measurements and plasma density characterization with the use of a triple Langumir probe. The results show that relevant plasma densities that match facility beam parameters are readily achievable.
    Electronic ISSN: 2410-390X
    Topics: Electrical Engineering, Measurement and Control Technology
    Published by Molecular Diversity Preservation International
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  • 6
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    The Future of Solar Power in the United Kingdom (2015)
    Molecular Diversity Preservation International
    Details
    Publication Date: 2015-07-30
    Electronic ISSN: 1996-1073
    Topics: Energy, Environment Protection, Nuclear Power Engineering
    Published by Molecular Diversity Preservation International
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  • 7
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    Replacing the Z-phenyl Ring in Tamoxifen® with a para-Connected NCN Pincer-Pt-Cl Grouping by Post-Modification † (2021)
    Molecular Diversity Preservation International
    Details
    Publication Date: 2021-03-26
    Description: Post-modification of a series of NCN-pincer platinum(II) complexes [PtX(NCN-R-4)] (NCN = [C6H2(CH2NMe2)2-2,6]–, R = C(O)H, C(O)Me and C(O)Et), X = Cl– or Br–) at the para-position using the McMurry reaction was studied. The synthetic route towards two new [PtCl(NCN-R-4)] (R = C(O)Me and C(O)Et) complexes used above is likewise described. The utility and limitations of the McMurry reaction involving these pincer complexes was systematically evaluated. The predicted “homo-coupling” reaction of [PtBr(NCN-C(O)H-4)] led to the unexpected formation of 3,3′,5,5′-tetra[(dimethylamino)methyl]-4,4′-bis(platinum halide)-benzophenone (halide = Br or Cl), referred to hereafter as the bispincer-benzophenone complex 13. This material was further characterized using X-ray crystal structure determination. The applicability of the pincer complexes in the McMurry reaction is shown to open a route towards the synthesis of tamoxifen-type derivatives of which one phenyl ring of Tamoxifen® itself is replaced by an NCN arylplatinum pincer fragment. The newly synthesized derivatives can be used as potential candidates in anti-cancer drug screening protocols. Two NCN-arylpincer platinum tamoxifen type derivatives, 5 and 6, were successfully synthesized and of 5 the separation of the diastereomeric E-/Z-forms was achieved. Compound 6, which is the pivaloyl protected NCN pincer platinum hydroxy-Tamoxifen® derivative, was obtained as a mixture of E-/Z-isomers. The new derivatives were further analyzed and characterized with 1H-, 13C{1H}- and 195Pt{1H}-NMR, IR, exact mass MS and elemental analysis.
    Electronic ISSN: 1420-3049
    Topics: Chemistry and Pharmacology
    Published by Molecular Diversity Preservation International
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  • 8
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    Deciphering the Influence of Electrolytes on the Energy Storage Mechanism of Vertically-Oriented Graphene Nanosheet Electrodes by Using Advanced Electrogravimetric Methods (2020)
    Molecular Diversity Preservation International
    Details
    Publication Date: 2020-12-07
    Description: Electrolyte composition is a crucial factor determining the capacitive properties of a supercapacitor device. However, its complex influence on the energy storage mechanisms has not yet been fully elucidated. For this purpose, in this study, the role of three different types of electrolytes based on a propylene carbonate (PC) solution containing tetrabutylammonium perchlorate (TBAClO4), lithium perchlorate (LiClO4) and butyltrimethylammonium bis(trifluoromethylsulfonyl)imide (N1114TFSI) ionic liquid on vertically-oriented graphene nanosheet electrodes has been investigated. Herein, in situ electrochemical quartz crystal microbalance (EQCM) and its coupling with electrochemical impedance spectroscopy (EIS), known as ac-electrogravimetry, have allowed the dynamic aspects of the (co)electroadsorption processes at the electrode-electrolyte interface to be examined. A major contribution of ClO4− anions (TBAClO4) was evidenced, whereas in the PC/N1114TFSI mixture (50:50 wt%) both anions (TFSI−) and cations (N1114+) were symmetrically exchanged during cycling. In the particular case of LiClO4, solvation of Li+ cations in PC was involved, affecting the kinetics of electroadsorption. These results demonstrate the suitability of dynamic electrogravimetric methods to unveil the interfacial exchange properties of mobile species for the conception of new high performance energy storage devices.
    Electronic ISSN: 2079-4991
    Topics: Physics
    Published by Molecular Diversity Preservation International
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  • 9
    Electronic Resource
    Electronic Resource
    Synthesis and interfacial behavior of poly(Lys-Tyr-Tyr-Lys) (1995)
    New York : Wiley-Blackwell
    Biopolymers 35 (1995), S. 629-637 
    Details
    ISSN: 0006-3525
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Poly(Lys-Tyr-Tyr-Lys) was synthesized by polycondensation of the tetrapeptide unit using paranitrophenyl esters. The conformation of poly (Lys-Tyr-Tyr-Lys) is very dependent on its environment. CD spectra in bulk are difficult to interpret owing to the contribution of Tyr residues, but from ir spectra it seems that poly(Lys-Tyr-Tyr-Lys) adopts preferentially an unordered conformation in water. Addition of salts induces a partial transition to a β structure. The behavior is different at interfaces. When poly(Lys-Tyr-Tyr-Lys) is spread as a film on a water subphase, the shape of the compression isotherm curves is compatible with a stacking of two β-sheets. On a KCl subphase, the polymer film is more expanded and more compressible, and the isotherm curve resembles that of a polymer in a random conformation. The analysis by CD and ir spectroscopy of transferred monolayers using the Langmuir-Blodgett technique allowed us to confirm and make these data more precise: on a water subphase the spectra are those of an antiparallel β structure. At the interface of a saline solution the spectra are compatible with a mixture of random coil (largely) and a small content of β structures. © 1995 John Wiley & Sons, Inc.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bip.360350609
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  • 10
    Electronic Resource
    Electronic Resource
    Topographic analysis of the S7 binding subsite of the tachykinin neurokinin-1 receptor (1996)
    New York : Wiley-Blackwell
    Biopolymers 39 (1996), S. 133-147 
    Details
    ISSN: 0006-3525
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Conformationally and configurationally restricted rotameric probes of phenylalanine have been incorporated in the sequence of substance P (SP) - Arg-Pro-Lys-Pro-Gln-Gln-Phe-Phe-Gly-Leu-Met-NH2 - for analyzing the binding pockets of Phe7 (S7) and Phe8 (S8), in the neurokinin-1 receptor. These analogues of phenylalanine are (2S, 3R)- and (2S, 3S)-indanylglycines, E- and Z-α, β-dehydrophenylalanines, and 2(S)-α, β-cyclopropylphenylalanines [ΔE Phe, ΔZPhe, ▿E2(S)Phe, and ▿Z2(S)Phe]. Binding data obtained with either conformationally (Ing diastereoisomers) or configurationally (ΔEPhe, ΔZPhe) probes have unveiled large differences in the binding potencies of these rotameric probes. With the support of nmr data and energy calculations done on these SP-substituted analogues, we attempt to answer questions inherent to such study. First, none of these six probes prevents the formation of bioactive conformation(s) of the backbone of SP. Second, both diastereoisomers (S, S) and (S, R) of indanylglycine preferentially adopt, in the sequence of SP, the gauche (-) and trans side-chain orientations, respectively, as previously postulated from energy calculations with model peptides. However, in solution, the difference in energy between these rotamers included in the sequence of SP, compared to model peptides, is smaller since the other rotamer can be detected in [(2S, 3R) Ing7]SP. Finally, from this study we can hypothesize that the large variations observed in the affinities of Phe7 substituted analogues of SP must come from steric hindrance in the S7 binding site, which drastically restricts the space filling around the Cα (SINGLE BOND) Cβ bond of residue 7. © 1996 John Wiley & Sons, Inc.
    Additional Material: 3 Ill.
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