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  • American Institute of Physics (AIP)  (173)
  • Emerald  (127)
  • 1995-1999  (300)
  • 1955-1959
  • 1996  (300)
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  • 1995-1999  (300)
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  • 11
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Physics of Plasmas 3 (1996), S. 8-9 
    ISSN: 1089-7674
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: In this Letter a useful and instructive form of the magnetohydrodynamic potential energy is presented. In this form all but one term is positive definite, each term is self-adjoint, and it can be directly evaluated numerically in nonorthogonal coordinate systems. The product of the local shear and the current parallel to the magnetic field is identified as a significant parameter for current-driven instabilities. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 12
    Digitale Medien
    Digitale Medien
    Woodbury, NY : American Institute of Physics (AIP)
    Chaos 6 (1996), S. 461-465 
    ISSN: 1089-7682
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: Dynamic behavior of the pH-regulated oscillations has been studied for the hydrogen peroxide oxidation of thiosulfate ions in the presence of trace amounts of copper(II) ions in a semibatch reactor. A solution of 0.08 M Na2S2O3 and 0.112 M NaOH was flowed at 0.160 mL/min into 300 mL of solution containing the H2O2 and Cu2+ in a vessel. There exists a critical value of the H2O2 or Cu2+ concentrations below which the system does not oscillate. The oscillations appear due to an infinite period bifurcation at low initial concentrations of the H2O2. The initial concentration of Cu2+ may be considered as a bifurcation parameter in this case. Increase of the initial hydrogen peroxide concentration causes the pH-regulated oscillations through a nondegenerate supercritical Hopf bifurcation. The classification of bifurcations is based on the analysis of the behavior of oscillation amplitude and period at different initial concentrations of the H2O2 and Cu2+. Our results show a possibility to distinguish different scenarios for the appearance of transient oscillations in semibatch experiments. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 13
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 3364-3365 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: We describe a method to collect x-ray absorption fine structure (XAFS) spectra of ions in a supercritical water solvent. Supercritical water (SCW), at temperatures above water's critical point of 374 °C, is an interesting solvent for chemical reactions and hazardous waste destruction due to the high solubility of organics and the aggressive oxidizing environment. XAFS may provide a better understanding of the solvent environment in SCW. The XAFS cell used in these studies was composed of a block of high-nickel alloy, Hastelloy C-22, containing two windows for transmission of the x-ray beam and a single optical view window. All internal wetted surfaces were platinum plated. The maximum operating conditions for this design were 500 °C and 700 bar. The x-ray transmission windows consisted of CVD (chemical vapor deposition) diamond windows (3 mm diameter ×0.5 mm thick) that were brazed to the tip of a standard 1/4-in. high-pressure, coned-shape fitting. Spectra are reported for strontium and rubidium ions in a supercritical water solvent. This cell design could be used for a variety of other solvent systems at high temperatures and high pressures. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 14
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 2890-2893 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: A spectrometer based on a dc superconducting quantum interference device (SQUID) has been developed for the direct detection of nuclear magnetic resonance (NMR) or nuclear quadrupole resonance (NQR) at frequencies up to 5 MHz. The sample is coupled to the input coil of the niobium-based SQUID via a nonresonant superconducting circuit. The flux locked loop involves the direct offset integration technique with additional positive feedback in which the output of the SQUID is coupled directly to a low-noise preamplifier. Precession of the nuclear quadrupole spins is induced by a magnetic field pulse with the feedback circuit disabled; subsequently, flux locked operation is restored and the SQUID amplifies the signal produced by the nuclear free induction signal. The spectrometer has been used to detect 27Al NQR signals in ruby (Al2O3[Cr3+]) at 359 and 714 kHz. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 15
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 3965-3972 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: We describe a time-domain (pulsed) eddy-current technique for determining the thickness and conductivity of conductive coatings on metal plates. The pulsed eddy-current instrument records the transient current induced in an absolute, air-cored coil placed next to a layered sample and excited with a step-function change in voltage. Signals are digitized with 16-bit resolution at a sampling rate of 1 megasamples per second, and the excitation is repeated at a rate of 1 kHz. The instrument displays the difference in the transient current measured on the substrate and on the substrate plus coating. We measured pulsed eddy-current signals for a series of metal foils of varying thickness placed over 1 cm thick metal plates. Seven combinations of foil and substrate metals were studied including pure aluminum, copper, and titanium foils over substrates of aluminum, titanium alloy, and stainless steel. We report results for three types of samples: aluminum foils on Ti–6Al–4V substrate, titanium foils on 7075 aluminum alloys, and aluminum foils on AISI 304 stainless steel. Foil thickness ranged from 0.04–1.00 mm. We found that three features of the signal—the peak height, the time of occurrence of the first peak, and a characteristic zero-crossing time—depend sensitively upon the thickness of the layers and the relative electrical conductivity of coating and substrate. Theoretical calculations were compared to the measurements. Absolute agreement between calculated and measured signals was, in most cases, within 3%. No calibration with respect to artifact standards was used. Finally, a feature-based rapid inversion method was developed and used to infer the thickness and conductivity of the layers. The accuracy of the inversion depends upon the thickness of the layer and the contrast in conductivity between layer and substrate. For the materials studied the thickness could be determined within 13%, while the error in determining conductivity was 20%–30%. The time-domain method is much simpler and hundreds of times faster than the frequency-domain method previously reported by Moulder et al. [Rev. Sci. Instrum. 63, 3455 (1992)]. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 16
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 3310-3319 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: This article describes the fabrication and operating principles of a device suitable for measuring displacements, stresses, strains, accelerations, and forces. The device consists of an elastomeric material with a surface relief diffraction grating embossed on its surface. Mechanical compression of this element changes the way that it diffracts light. This article also describes designs and performance characteristics of simple accelerometers and pressure sensors based on these devices. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 17
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 2738-2751 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: An apparatus for measuring absolute cross sections due to electron-impact excitation out of the metastable levels of rare-gas atoms via the optical method is described with the focus specifically on excitation out of the 2 3S metastable helium level. The metastable helium target (He*) is prepared by charge exchange between 1.6 keV He+ ions and cesium vapor. An electron beam crosses the fast metastable beam target at a right angle and the fluorescence is collected at right angles to both beams. The charge transfer reaction produces He atoms mainly in the n=2 He levels. Because the target contains a negligible ground state He fraction, we can measure excitation cross sections from excitation threshold up to an arbitrarily high energy (keV regime) which represents a major improvement over previous metastable excitation cross sections measurements. The He* target density is extremely small (∼106 atoms/cm3) yielding minuscule signal rates. We describe steps taken to maximize the signal-to-noise ratio. We discuss the implications of using a fast beam target including both the finite flight time of the excited atoms across the light gathering region and the reduction of the cascade contributions to the apparent cross sections. A discussion of the identification and elimination of various systematic effects is also given. To measure absolute cross sections, we explicitly determine the spatial distributions of both the electron and metastable beams, as well as the spatially dependent response of the fluorescence gathering region. We determine the absolute flux of fast metastable atoms using a thermal detector calibrated with a He+ ion beam. As examples, we present absolute cross sections for excitation out of the 2 3S metastable level into the 3 3D and 4 3D levels. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 18
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 2843-2845 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: A method is described to acquire x-ray absorption fine structure (XAFS) spectra of high-pressure liquid and supercritical fluid solutions. The technique employs a short length of fused-silica capillary tubing that has an inner diameter of 250 μm and an outer diameter of 360 μm. A hairpin bend is formed near the center of the capillary and the bend is then placed end-on directly in the focused x-ray beam. Fluorescence spectra were acquired in a 90° geometry using a 13 element Ge detector. Demonstration XAFS spectra are reported for a Mn organometallic complex dissolved in subcritical and supercritical CO2. Although the maximum pressure of these studies was 160 bar, with slight modification, the method will be applicable to studies requiring pressures as high as 4 kbar. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 19
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 2251-2256 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: Conversion of an electron microprobe for use as an x-ray microtomograph is described. Only minor modifications are required, indeed several of the utilities of the microprobe can be used to ensure high resolution radiography and tomography. System performance was evaluated by analysis of glass fiber reinforced polymer composites and of a carbonate reservoir rock. Individual glass fibers of 10 and 20 μm diameter are clearly visible in the former. In the latter, comparison with scanning electron micrographs shows reliable reconstruction of external morphology. In addition, internal pore structure can be studied a posteriori using the tomography data. Spatial resolutions in radiography of better than 3 μm and in tomography of 10 μm have been demonstrated. Further improvements to the detector system and increased data handling capacity are possible to achieve 1 μm resolution tomographic images. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 20
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 3352-3352 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: The high heat load at the surfaces of the first x-ray optical elements at the APS requires special measures to be taken to more completely utilize the beam. A conceptually new design for such an element, proposed, realized, and tested by M. Hart and conveniently called "matchbox,'' is to be implemented at the IMCA-CAT BM beamline as the first monochromator crystal. The requirements of the IMCA-CAT companies for the BM beamline dictate that an optimization of the design is made for a given x-ray energy range E=13 keV ±1 keV. A modification of the original design to improve the vacuum compatibility of the device was made in collaboration with M. Hart. A FEA optimization of the geometry is made using the ALGOR and ABAQUS programs. Determination of the resulting slopes and the useful crystal surface after the best compensation of the thermal distortions are also made. The surface profile obtained by the FEA study was used to perform a ray-tracing analysis of the IMCA-CAT BM beamline. The results of the ray-tracing study will be presented. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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