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  • Chemistry  (16)
  • Polymer and Materials Science  (7)
  • Engineering General
  • 1990-1994  (17)
  • 1993  (17)
  • 1
    Electronic Resource
    Electronic Resource
    Synthesis of uniform poly(aspartic acids) (1993)
    New York : Wiley-Blackwell
    Die Makromolekulare Chemie 194 (1993), S. 1095-1104 
    Details
    ISSN: 0025-116X
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Poly(aspartic acids) of different chain lengths (11, 14, 18, 24, 30, 52, 58, ≈ 115) were prepared, for the use in aminoglycoside-induced nephrotoxicity inhibition studies, some in their pure L- or D-configuration and in pure α-linkage form by the polymerization of α-amino acid N-carboxyanhydride (NCA) derivatives with a variety of dialkyl aspartate molecules as primary amine initiators. The primary amine chosen served as an internal reference in the 1H NMR spectrum for the estimation of the degree of polymerization (chain length) in these molecules. Poly(aspartic acids) with varying amounts of D and L asymmetric centres and in pure α-linkage from were also prepared. Poly[(α-co-β)(L-co-D) aspartic acid] was prepared by a simplified thermal polymerization procedure for biological studies and also to study the tacticity effects in its 13C NMR spectrum. A qualitative correlation was demonstrated between the retention times from gel-permeation chromatographic analysis and the 1H NMR method used to estimate the polymer chain length.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/macp.1993.021940405
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  • 2
    Electronic Resource
    Electronic Resource
    Effect of nonlinear bisphenol A units on the liquid crystalline properties of poly(2-phenylhydroquinone terephthalate) (1993)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part A: Polymer Chemistry 31 (1993), S. 283-285 
    Details
    ISSN: 0887-624X
    Keywords: liquid crystalline polymers ; liquid crystalline polyesters ; bisphenol A copolymers ; thermotropic copolyesters ; phenylhydroquinone copolyesters ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 2 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pola.1993.080310134
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  • 3
    Electronic Resource
    Electronic Resource
    Catalytic and interfacial aspects of enzymatic polymer synthesis in reversed micellar systems (1993)
    New York, NY [u.a.] : Wiley-Blackwell
    Biotechnology and Bioengineering 41 (1993), S. 531-540 
    Details
    ISSN: 0006-3592
    Keywords: horseradish peroxidase ; reversed micelles ; phenolic polymers ; enzyme kinetics ; Chemistry ; Biochemistry and Biotechnology
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Biology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: The enzyme horseradish peroxidase, when encapsulated in reversed micelles, is capable of catalyzing the synthesis of phenolic and aromatic amine polymers. The synthesis of polyethylphenol is specifically considered in this article and is found to be extremely feasible in the micellar system. Polymer chain growth can be controlled to some degree by manipulating the ability of the solvent to sustain chain solubility; this is effectively done by adjusting the surfactant concentration. This results in a degree of control of polymer molecular weight. The synthesized polymer drops out of solution and can be easily recovered. © 1993 John Wiley & Sons, Inc.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bit.260410505
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  • 4
    Electronic Resource
    Electronic Resource
    Effect of energy distribution on sorption kinetics in bidispersed particles (1993)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 39 (1993), S. 249-261 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: In this article, we present a model to describe sorption kinetics of gaseous adsorbates onto bidispersed heterogeneous microporous particles. This model describes adsorption and desorption of gaseous adsorbates with allowance for the energy distribution of adsorption site for both equilibrium isotherm and diffusion of the adsorbed species. The adsorbed species of all energy level diffuse in two directions inside the particle. One direction is the direction along the particle coordinate while the other is the direction perpendicular to the particle coordinate (that is, the direction into the grain of the solid). This model is more fundamental than models previously proposed by Do and coworkers. Effects of energy distribution on the adsorption and desorption dynamics are investigated. Extensive experimental analysis of adsorption and desorption dynamics of ethane and propane onto Ajax activated carbon are carried out to validate this theory.
    Additional Material: 10 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690390207
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  • 5
    Electronic Resource
    Electronic Resource
    Parametric study on the bulk hydraircooling of spherical food products (1993)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 39 (1993), S. 1870-1884 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: A numerical study of the bulk hydraircooling of spherical food products is performed using the technique of spraying chilled water to form a thin film over the food products while blowing cold unsaturated air in the countercurrent or cocurrent direction. This precooling process is found to combine the advantages of hydro-and air cooling.Governing equations describing the simultaneous heat and mass transfer occurring in the hydraircooling process for both counterflow and parallel-flow arrangements are solved using finite-difference numerical methods. A parametric study is performed to determine the effect of important processing parameters on the process time. It is generally observed that higher quantities of spray water, air-mass flow rate and product thermal conductivity, as well as lower values of water temperature will result in faster rates of cooling. For the same operating conditions, parallel-flow arrangement leads to higher plant capacities.
    Additional Material: 18 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690391114
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  • 6
    Electronic Resource
    Electronic Resource
    A general method of designing gas and gas-liquid injectors using laws of turbulent jet mixingPaper presented at the “Jahrestreffen der Verfahrens-Ingenieure”, Cologne, 25-27 Sept. 1991. (1993)
    Weinheim : Wiley-Blackwell
    Chemical Engineering & Technology - CET 16 (1993), S. 94-101 
    Details
    ISSN: 0930-7516
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Based on the equation for entrainment of a turbulent free jet, a simple method of designing gas and gas-liquid injectors is presented. Using the formula for mass flow ratio of an injector consisting of a nozzle and a short cylindrical mixing tube open at both ends, a general equation for designing any injector with variable geometry and flow resistances is given. The optimization procedure is outlined. Compared to the conventional design of injectors, starting from macroscopic mass and momentum balances, the present method is much simpler, easily applicable and involves only one empirical entrainment coefficient. It is particularly advantageous in the case of variable density of the motive and entrained fluids since the density ratio appears explicitly in the relevant equations.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/ceat.270160205
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  • 7
    Electronic Resource
    Electronic Resource
    Monitoring the levels of chloroacetic acids in the industrial environment by high performance liquid chromatographyIICT Communication no. 3145 (1993)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 16 (1993), S. 381-383 
    Details
    ISSN: 0935-6304
    Keywords: Reversed phase LC ; Industrial contaminants ; Chloroacetic acids ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240160611
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  • 8
    Electronic Resource
    Electronic Resource
    A new 3-D finite element model to evaluate added mass for analysis of fluid-structure interaction problems (1993)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 36 (1993), S. 997-1012 
    Details
    ISSN: 0029-5981
    Keywords: Engineering ; Engineering General
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: The paper presents the results of investigations conducted to evaluate the added mass to represent fluid-structure interaction effects in vibration/dynamic analysis of floating bodies such as ship hulls. While the structural plating is idealized by 9-noded plate/shell finite elements, the fluid domain is modelled by 20-noded/21-noded 3-D finite elements in the investigations conducted. A new 8-noded element has been developed to model the interface between the structure and the fluid. An efficient computational methodology has been used for computation of added mass. The finite element models are validated by comparing the results with those given by analytical solution for a submerged sphere. The efficacy of the finite element model is demonstrated through convergence of the results obtained for a floating barge problem. A better convergence rate and distribution of added mass in three orthogonal directions have been obtained.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/nme.1620360608
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  • 9
    Electronic Resource
    Electronic Resource
    Electron-impact-induced Ortho effects in (O-carboxyphenyl)diphenylphosphineIICT Communication No. 3084. (1993)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 28 (1993), S. 267-270 
    Details
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Proximity effects of the carboxyl group with the phosphorus atom in the molecular ion of (o-carboxyphenyl)diphenylphosphine (1) leads to the loss of ĊHO to form the base peak at m/z 277, which is totally absent in the (m- and p-carboxyphenyl)diphenylphosphines. The mechanism of the loss of ĊHO and the fragmentation of 1 was investigated in detail using metastable ion, collision-induced dissociation and high-resolution studies.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/oms.1210280320
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  • 10
    Electronic Resource
    Electronic Resource
    Improving graft level during photoinduced graft-copolymerization of styrene onto cotton cellulose (1993)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 49 (1993), S. 1423-1430 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Styrene was graft-copolymerized onto cotton cellulose using photoinitiators uranyl nitrate (UN), ceric ammonium nitrate (CAN), and benzoin ethyl ether (BEE) under ultraviolet radiation. UN gave somewhat higher graft add-on. Preswelling of the substrate or using divinyl benzene in the grafting bath gave an increased level of graft, the later technique being more efficient. The moisture regain and tenacity decreased, whereas thermal stability increased in proportion to the graft add-on. © 1993 John Wiley & Sons, Inc.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1993.070490810
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