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  • ASTROPHYSICS  (8)
  • Polymer and Materials Science  (3)
  • Astrophysics
  • 1990-1994  (11)
  • 1993  (5)
  • 1992  (6)
Collection
Keywords
Publisher
Years
  • 1990-1994  (11)
Year
  • 1
    Electronic Resource
    Electronic Resource
    Synthesis and characterization of oligocyclosiloxanes via the hydrosilation of vinylsilanes and vinylsiloxanes with heptamethylcyclotetrasiloxane (1993)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part A: Polymer Chemistry 31 (1993), S. 891-900 
    Details
    ISSN: 0887-624X
    Keywords: oligocyclosiloxanes ; hydrosilation ; heptamethylcyclotetrasiloxane ; siloxane redistribution ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The preparation of oligocyclosiloxanes via hydrosilation reactions has been investigated. Hydrosilation reactions employing heptamethylcyclotetrasiloxane and vinyl-containing silanes and siloxanes yielded a variety of oligocyclosiloxanes with various numbers of cyclosiloxane rings connected through tri-, tetra-, penta-, hexa-, hepta-, or octafunctional junctions. The oligocyclosiloxanes were characterized by gas chromatography, IR spectroscopy, 29Si-, 1H-, and 13C-NMR spectroscopy, elemental analysis, and vapor phase osmometry. The polycyclics were redistributed with hexamethyldisiloxane and the resulting fragments analyzed by gas chromatography. All results were consistent with the formation of isomeric oligocyclosiloxanes due to a lack of absolute regioselectivity of the hydrosilation reaction. © 1993 John Wiley & Sons, Inc.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pola.1993.080310407
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  • 2
    Electronic Resource
    Electronic Resource
    Tissue response and in vivo degradation of selected polyhydroxyacids: Polylactides (PLA), poly(3-hydroxybutyrate) (PHB), and poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHB/VA)The opinions or assertions about specific products identified by brand name contained herein are the private views of the authors (JGD, MKH) and are not to be construed as conveying either an official endorsement or criticism by the U.S. Department of Health and Human Services or the Food and Drug Administration. (1993)
    Hoboken, NJ : Wiley-Blackwell
    Journal of Biomedical Materials Research 27 (1993), S. 1135-1148 
    Details
    ISSN: 0021-9304
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Medicine , Technology
    Notes: The tissue response and in vivo molecular stability of injection-molded polyhydroxyacids - polylactides (PLA), poly(3-hydroxybutyrate) (PHB), and poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHB/VA, 5-22% VA content) - were studied. Polymers were implanted subcutaneously in mice and extirpated at 1, 3, and 6 month in order to study tissue response and polymer degradation.All polymers were well tolerated by the tissue. No acute inflammation, abscess formation, or tissue necrosis was observed in tissues adjacent to the implanted materials. Furthermore, no tissue reactivity or cellular mobilization was evident remote from the implant site. Mononuclear macrophages, proliferating fibroblasts, and mature vascularized fibrous capsules were typical of the tissue response. Degradation of the polymers was accompanied by an increase in collagen deposition. For the polylactide series, the inflammatory response after 1 month of implantation was less for materials containing the D-unit in the polymer chain, whereas in the case of the polyhydroxybutyrate/valerates, the number of inflammatory cells increased with increasing content of the valerate unit in the polymer chain. Between 1-3 months, there was slightly more tissue response to the PHB and PHB/VA polymers than to PLA. This response is attributed to the presence of leachable impurities and a low molecular weight soluble component in the polyhydroxybutyrate/valerates. At 6 months, the extent of tissue reaction was similar for both types of polymers.All polylactides degraded significantly (56-99%) by 6 months. For a poly(L-lactide) series, degradation rate in vivo decreased with increasing initial molecular weight of the injection-molded polymer. Several samples showed pronounced bimodal molecular weight distributions (MWD), which may be due to differences in degradation rate, resulting from variability in distribution of crystalline and amorphous regions within the samples. This may also be the result of two different mechanisms, i.e., nonenzymatic and enzymatic, which are involved in the degradation process, the latter being more extensive at the later stage of partially hydrolyzed polymer. The PHB and PHB/VA polymers degraded less (15-43%) than the polylactides following 6 months of implantation. Generally, the polymer with higher valerate content (19%, 22% degraded most. The decrease in molecular weight was accompanied by a narrowing of the MWD for PHB and copolymers; there was no evidence of a bimodal MWD, possibly indicating that the critical molecular weight that would permit enzyme/polymer interaction had not been reached. Weight loss during implantation ranged from 0-50% for the polylactides, whereas for the PHB polymers weight loss ranged from 0-1.6%. © 1993 John Wiley & Sons, Inc.
    Additional Material: 13 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jbm.820270904
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  • 3
    Electronic Resource
    Electronic Resource
    Improved fire safety of composites for naval applications (1992)
    New York, NY [u.a.] : Wiley-Blackwell
    Fire and Materials 16 (1992), S. 119-125 
    Details
    ISSN: 0308-0501
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Architecture, Civil Engineering, Surveying , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: This study is based on the use of integral, hybrid thermal barrier to protect the core of the composite structure. Thermal barrier treatments evaluated in this study include ceramic fabric, ceramic coating, intumescent coating, hybrid of ceramic and intumescent coating, silicone foam, and phenolic skin. The composite systems evaluated in combination with thermal barrier treatments included glass/vinyl ester, graphite/epoxy, graphite/bismaleimide, and graphite/phenolic. All configurations were tested for flammability characteristics. These included smoke density and combustion gas generation (ASTM E-662), residual flexural strength (ASTM D-790), heat release rate, and ignitability (ASTM E-1354). ASTM E-662 test method covers the determination of specific optical density of smoke generated by solid materials. ASTM D-790 test method covers the determination of flexural properties of composite materials in the form of rectangular bars. ASTM E-1354 (cone calorimeter) covers the measurement of the response of materials exposed to controlled levels of radiant heating with or without an external ignitor, and is used to determine the ignitability, heat release rates, mass loss rates, effective heat of combustion, and visible smoke development. Without any fire barrier treatments, all composite systems evaluated in this study failed to meet ignitability and peak heat release requirements of MIL-STD-2031 (SH) at radiant heat fluxes of 75 and 100 kW m-2, respectively. Intumescent coating and a hybrid system consisting of intumescent coating over ceramic coating were the most effective fire barrier treatments for composite systems evaluated in this study. Using either of these treatments, all composite systems met the ignitability requirements of 90 and 60 at 75 and 100 kW m-2, respectively. Except for glass/vinyl ester, all systems also met the peak and average heat release requirements of MIL-STD-2031 (SH) at radiant heat fluxes of 25, 75, and 100 kW m-2, respectively.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/fam.810160303
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  • 4
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    The spatial distribution of large cometary meteoroids in the inner solar system (1992)
    In:  CASI
    Details
    Publication Date: 2013-08-31
    Description: A model of the spatial density distribution of large (m greater than 10(exp -3) g) cometary meteoroids in the inner solar system is obtained assuming that they have orbits closely associated with that of their parent comet. Distributions of the orbital parameters of the Taurid, Quadrantid and Perseid meteoroid streams are used in developing the model.
    Keywords: ASTROPHYSICS
    Type: Lunar and Planetary Inst., Asteroids, Comets, Meteors 1991; p 403-406
    Format: application/pdf
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  • 5
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    CCD imaging of the inner coma jets of comet P/Halley (1992)
    In:  CASI
    Details
    Publication Date: 2013-08-31
    Description: We analyze the inner coma section of a CCD image of comet P/Halley taken at 1807 UT on 13 March 1986 using a C2 filter (wavelength 5000 to 5200A, half maximum) with the 3.8 m Anglo Australian Telescope at Siding Springs, Australia. Atmospheric turbulence leads to a spreading of the image detail and this produces a blander image of the inner coma region with a slower radial decrease of brightness in comparison to the unaffected image. We remove this smearing by utilizing the point spread function of a star on the same CCD image. Jets were then revealed by removing the average background. Analysis of the jet structure enabled us to estimate the lower limit of the parent molecule velocity. This is found to be 0.3 km s(exp -1).
    Keywords: ASTROPHYSICS
    Type: Lunar and Planetary Inst., Asteroids, Comets, Meteors 1991; p 89-92
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  • 6
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    A2163 - An exceptionally hot cluster of galaxies (1992)
    In:  Other Sources
    Details
    Publication Date: 2019-07-12
    Description: The X-ray spectrum of the distant galaxy cluster A2163 was measured in the energy range 1-18 keV with the Ginga satellite. A combined analysis of these data with data previously obtained with the Einstein Observatory is presented. The mean temperature and X-ray luminosity derived are exceptionally high compared to other clusters: kT = 12.9 keV, L(x) (2-10 keV) = 3.5 x 10 exp 45 ergs/s for z = 0.15, as are the gas mass (6.7 x 10 exp 14 solar mass) and binding mass (25 x 10 exp 14 solar mass). The very existence of such a cluster can provide interesting constraints on the relative distribution of 'visible' mass and dark matter, an important parameter in cold dark matter models for formation of structure in the universe.
    Keywords: ASTROPHYSICS
    Type: Astrophysical Journal, Part 1 (ISSN 0004-637X); 390; 2 Ma; 345-349
    Format: text
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  • 7
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    Semiempirical limits on the thermal conductivity of intracluster gas (1992)
    In:  Other Sources
    Details
    Publication Date: 2019-07-12
    Description: A semiempirical method for establishing lower limits on the thermal conductivity of hot gas in clusters of galaxies is described. The method is based on the observation that the X-ray imaging data (e.g., Einstein IPC) for clusters are well described by the hydrostatic-isothermal beta model, even for cooling flow clusters beyond about one core radius. In addition, there are strong indications that noncooling flow clusters (like the Coma Cluster) have a large central region (up to several core radii) of nearly constant gas temperature. This suggests that thermal conduction is an effective means of transporting and redistributing the thermal energy of the gas. This in turn has implications for the extent to which magnetic fields in the cluster are effective in reducing the thermal conductivity of the gas. Time-dependent hydrodynamic simulations for the gas in the Coma Cluster under two separate evolutionary scenarios are presented. One scenario assumes that the cluster potential is static and that the gas has an initial adiabatic distribution. The second scenario uses an evolving cluster potential. These models along with analytic results show that the thermal conductivity of the gas in the Coma Cluster cannot be less than 0.1 of full Spitzer conductivity. These models also show that high gas conductivity assists rather than hinders the development of radiative cooling in the central regions of clusters.
    Keywords: ASTROPHYSICS
    Type: Astrophysical Journal, Part 1 (ISSN 0004-637X); 394; 2 Au; 452-458
    Format: text
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  • 8
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    An astrophysics data program investigation of spatial structure of supernova remnants (1993)
    In:  CASI
    Details
    Publication Date: 2019-07-13
    Description: The final report on astrophysics data program investigation of spatial structure of supernova remnants for the period 1 Aug. 1989 to 31 Jul. 1991 is presented. The goal of the project was the study of the spatial structure of supernova remnants (SNR's) as observed in the x-ray band. A number of software tools were developed for the analysis: (1) a program to fit various geometric models to high resolution x-ray data, and (2) programs for Fourier Transform analysis of clumping in SNR's. These programs were applied to high resolution imager (HRI) data on the young galactic SNR's Tycho and Kepler with some success.
    Keywords: ASTROPHYSICS
    Type: NASA-CR-193104 , NAS 1.26:193104
    Format: application/pdf
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  • 9
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    Ginga observations of the Coma cluster and studies of the spatial distribution of iron (1993)
    In:  Other Sources
    Details
    Publication Date: 2019-07-13
    Description: The large area counters on the Japanese satellite Ginga have been used to determine the X-ray spectrum from the central region of the Coma cluster of galaxies over the energy range from 1.5 to 20 keV. The spectrum is well represented by an isothermal model of temperature 8.21 +/- 0.16 keV and a heavy element (iron) abundance of 0.212 +/- 0.027, relative to the cosmic value. The Ginga spectrum was found to be consistent with the X-ray spectra from the Tenma and EXOSAT satellites for a large class of nonisothermal temperature distributions. The measured iron elemental abundances were used to set a lower limit on the total mass of iron in Coma under the assumption that the iron is not distributed uniformly throughout the cluster. The mass ratio of iron relative to hydrogen (within 2 Mpc) is not less than 18 percent of the cosmic iron to hydrogen mass ratio. This compares to an average abundance of 24 percent if the iron is distributed uniformly. We discuss these results in terms of models for the production of iron in galaxy clusters.
    Keywords: ASTROPHYSICS
    Type: Astrophysical Journal, Part 1 (ISSN 0004-637X); 404; 2; p. 611-619.
    Format: text
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  • 10
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    The X-ray spectrum of Abell 665 (1992)
    In:  Other Sources
    Details
    Publication Date: 2019-07-12
    Description: The X-ray spectrum of the Abell 665 cluster of galaxies has been determined by the Ginga satellite. The spectrum can be well fitted by an isothermal model with kT = 8.26(+0.95; -0.81) keV and metal abundance 0.49 +/- 0.16. Joint analysis with lower energy spectral data from the Einstein Observatory is used to constrain the temperature distribution in the cluster. For a particular form of the polytropic temperature model we find the best fit to be the isothermal case, and we set an upper limit on the polytropic index of 1.35 (99-percent confidence). The virial mass of the cluster has been determined from both the X-ray data and the galaxy velocity dispersion. The mass estimates from the optical and X-ray analyses are fully consistent with each other. Abell 665 is found to be 0.82(+0.41; -0.26) times as massive as Coma if the two clusters are assumed to have the same spatial distribution of virial mass.
    Keywords: ASTROPHYSICS
    Type: Astrophysical Journal, Part 1 (ISSN 0004-637X); 398; 1; p. 62-68.
    Format: text
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