ISSN:
0749-1581
Keywords:
Solid-state NMR
;
Aminophosphonic acids
;
Crystallography
;
Shielding tensors
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
High-resolution 31P, 15N and 13C NMR spectra have been obtained for nine solid aminophosphonic acids under conditions of high-power decoupling, cross-polarization and magic-angle spinning. The NMR evidence shows that the asymmetric unit is a single molecule in all cases, which is consistent with the available diffraction studies. Phosphorus-31 shielding tensor components determined from static and slow-spinning MAS spectra are given for a number of the compounds.
Additional Material:
5 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260270509
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