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  • ASTROPHYSICS  (1)
  • Alkali flame ionization detection (AFID)  (1)
  • Condensed Matter: Electronic Properties, etc.
  • DDR
  • 1985-1989  (2)
  • 1986  (2)
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  • 1985-1989  (2)
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  • 1
    Electronic Resource
    Electronic Resource
    Quantitative analysis of ethylenediamine in plasma by capillary column gas chromatography (1986)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 9 (1986), S. 548-554 
    Details
    ISSN: 0935-6304
    Keywords: Gas liquid chromatography (GLC) ; Fused silica capillary columns ; Alkali flame ionization detection (AFID) ; Mass spectrometry (MS) ; Quantitation in human serum ; Ethylenediamine ; Aminophylline ; Small molecular weight amines and diamines ; m-Toluoyl derivatives ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A specific and sensitive method for the determination of ethylenediamine in human plasma is described. The aqueous sample is treated with m-toluoyl chloride, yielding the N,N′-bis(m-toluoyl) derivative of the diamine, which is extracted into dichloromethane and quantitated after “on column” methylation by capillary gas liquid chromatography with alkali flame ionization detection. The corresponding derivative of putrescine serves as internal standard. The assay is reproducible and calibration curves are linear over the concentration range 0.05 to 10 μg · ml-1. The lower detection limit is about 10 ng · ml-1. The structures of the compounds of interest eluting from the capillary column are examined by gas liquid chromatography/mass spectrometry. The assay has been applied to the analysis of ethylenediamine in plasma following the administration of aminophylline and ethylenediamine in a cross-over study to patients with bronchopulmonary diseases. The method also proves suitable for measuring other primary and secondary amines and diamines in aqueous solutions by gas liquid chromatography.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240091002
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    Paper (German National Licenses)
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  • 2
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    Spectroscopic CCD surveys for quasars at large redshift. I - A deep PFUEI survey (1986)
    In:  Other Sources
    Details
    Publication Date: 2019-07-12
    Description: A survey for faint quasars has been conducted using slitless spectroscopy with the PFUEI at the 200 inch (5 m) telescope. The survey covers a total of 0.91 sq deg in 113 fields at galactic latitudes above 30 deg. Calibrated spectra in the range 4500-7200 A were obtained for more than 9000 objects. Emission-line candidates were selected on the basis of two criteria: the equivalent width must exceed 50 A, and the signal-to-noise ratio of the detection of the line versus the sky background should be larger than 7. Among 45 candidates so selected, subsequent slit spectroscopy confirmed 27 emission-line objects. Among these, 17 are emission-line galaxies with redshifts in the range 0.04-0.31, and 10 are quasars with redshifts between 0.91 and 2.66. The well-defined selection criteria for these objects, together with the distribution of rest frame equivalent widths of the emission lines, allow derivation of the area of sky covered as a function of the continuum limiting magnitude. The observed number of quasars in the redshift range 0.7-2.7 agrees well with that predicted by the luminosity function models published by Schmidt and Green in 1983. It is concluded that quasars with an absolute magnitude of M(B) = -25 suffer a redshift cutoff near or below a redshift of 3.
    Keywords: ASTROPHYSICS
    Type: Astrophysical Journal, Part 1 (ISSN 0004-637X); 306; 411-427
    Format: text
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