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  • Analytical Chemistry and Spectroscopy  (59)
  • SPACE RADIATION  (41)
  • Humans
  • 1975-1979  (100)
  • 1975  (100)
  • 1
    Electronic Resource
    Electronic Resource
    The identification of 6-methoxy 8-aminoquionoline as a metabolite of primaquine in man (1975)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 2 (1975), S. 304-306 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The identification of 6-methoxy 8-aminoquinoline as a metabolite of Primaquine, an important antimalarial drug, is described. The metabolite is present in urine, plasma and erythrocytes following drug ingestion. It was identified by mass fragmentography of its 1H and 2H acetate and the acetate produced from authentic material. No evidence of further metabolites was obtained.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200020605
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    Analysis of carotenoids by field desorption mass spectrometry (1975)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 10 (1975), S. 1102-1110 
    Details
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The mass spectra of a variety of authentic carotenoids covering a range of structural types have been studied using the field desorption technique. All the compounds examined show the molecular ion as the base peak, even where this ion is of very low intensity in the electron-impact spectra. Little fragmentation is observed, but thermal decomposition can be induced in certain cases by using higher emitter currents. Application to a simple mixture of authentic compounds and a more complex mixture of sedimentary origin shows the potential of the method in the rapid qualitative screening of carotenoids in crude extracts.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/oms.1210101207
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    Paper (German National Licenses)
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  • 3
    Electronic Resource
    Electronic Resource
    Nuclear magnetic resonance and the conformation of some derivatives of Michler's ketone (1975)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 7 (1975), S. 154-159 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: 1H NMR spectra are reported for Michler's ketone and twenty of its derivatives, along with 13C chemical shifts for five of the compounds. 1H chemical shifts show only small changes with increasing substitution at the sterically hindered 2-position. Estimates of the dihedral angle between the benzene ring and C—CO—C planes have been obtained from the chemical shifts of C=O and 4-C for ketones 1, 3, 5, 15 and 16. These angles are both internally consistent and very similar to dihedral angles determined by other methods for corresponding compounds in the benzophenone series.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270070403
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  • 4
    Electronic Resource
    Electronic Resource
    The atomic number dependence of the X-ray continuum intensity and the practical calculation of background in energy dispersive electron microprobe analysis (1975)
    New York, NY [u.a.] : Wiley-Blackwell
    X-Ray Spectrometry 4 (1975), S. 149-156 
    Details
    ISSN: 0049-8246
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: Computer fitting techniques have been used to derive a new expression for the relationship between X-ray continuum intensity and atomic number for a range of electron acelerating potentials up to 25 kV, continuum energies up to 10 keV and average atomic numbers up to thirty. A practical approach to background corrections in energy dispersive electron microprobe analysis, which utilizes this expression, is outlined. The procedure should lead to significant improvements in both accuracy and detection limits in this method of X-ray analysis.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/xrs.1300040311
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  • 5
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    High-energy galactic gamma radiation from cosmic rays concentrated in spiral arms (1975)
    In:  Other Sources
    Details
    Publication Date: 2011-08-16
    Description: A model for the emission of high-energy (exceeding 100 Mev) gamma-rays from the galactic disk has been developed and compared with recent SAS-2 observations. In the calculation, it is assumed that (1) the high energy galactic gamma-rays result primarily from the interaction of cosmic rays with galactic matter, (2) the cosmic-ray density is proportional to the matter density on the scale of galactic arms, and (3) the matter in the Galaxy is distributed in a spiral pattern consistent with density-wave theory and experimental data on the matter distribution that is available, including the 21-cm H I line emission, continuum emission from H II regions, and data currently being used to estimate the H2 density. The calculated galactic-longitude distribution of gamma rays is in good agreement with the SAS-2 observations in relative shape and absolute flux. As a corollary, the nonuniform cosmic-ray distribution of this model tends to support the galactic origin of the fraction of cosmic rays which is important in the production of high-energy photons. Modifications of the basic model show that the gamma-ray flux is relatively sensitive to large variations of the assumed distribution of molecular hydrogen in the Galaxy.
    Keywords: SPACE RADIATION
    Type: Astrophysical Journal; 199; July 1
    Format: text
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  • 6
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    On emission lines in the cosmic gamma-ray background (1975)
    In:  Other Sources
    Details
    Publication Date: 2019-06-27
    Description: The composite spectrum of gamma-rays is calculated which results from the decay of Ni-56 to Co-56 to Fe-56 throughout the history of the universe. The results for several cosmological models are presented and compared with the Apollo 15 measurements at low resolution of the cosmic background. The radioactivity background is a significant fraction of the total, and several of its features may be detectable.-
    Keywords: SPACE RADIATION
    Type: Astrophysical Journal; 198; June 1
    Format: text
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  • 7
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    Cosmic ray intensity variations during 0200-0700 UT, August 5, 1972 (1975)
    In:  Other Sources
    Details
    Publication Date: 2019-06-27
    Description: The cosmic ray intensity variations over the energy range of about 0.5 MeV to 1 GeV during the early part of August 5 are discussed in relation to the intensity changes during the entire period of activity (August 2 to 11). Measurements of the interplanetary magnetic field and particle data from ground-based neutron monitors, lunar sensors, and detectors in board Explorers 41 and 43 are used in the investigation. Analysis is made of intensity changes during the period from 0200 to 0700 UT on August 5, the north-south asymmetry in neutron monitor intensities, changes in the alpha particle/proton flux ratios, the lag in onset times as recorded by the two Explorers, and observations of flux enhancement by the lunar detectors. The results indicate that the enhanced particle fluxes (about 1 GeV) were due to a leakage of galactic cosmic rays into a low-intensity region of the interplanetary magnetic field bounded by tangential discontinuities, which connected to different particle sources both near the sun and in the outer solar system.
    Keywords: SPACE RADIATION
    Type: Journal of Geophysical Research; 80; May 1
    Format: text
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  • 8
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    A cosmic gamma-ray burst on May 14, 1975 (1975)
    In:  CASI
    Details
    Publication Date: 2019-06-27
    Description: A cosmic gamma-ray burst is reported that occurred at 29309.11 s UTC, May 14, 1975. The burst was detected at an atmospheric depth of 4 g/sq cm residual atmosphere with the University of California double scatter gamma-ray telescope launched on a balloon from Palestine, Texas at 1150 UTC, May 13, 1975. The burst was observed both in the single scatter mode by the top liquid scintillator tank in anti-coincidence with the surrounding plastic scintillator and in the double scatter mode from which energy and directional information are obtained. The burst is 24 standard deviations above the background for single scatter events. The total gamma-ray flux in the burst, incident on the atmosphere with photon energy greater than 0.5 MeV, is 0.59 + or - 0.15 photons/sq cm. The initial rise time to 90% of maximum is 0.015 + or - 0.005 s and the duration is 0.11 s. Time structure down to the 5 ms resolution of the telescope is seen. The mean flux over this time period is 5.0 + or - 1.3 photons/sq cm/s and the maximum flux is 8.5 + or - 2.1 photons/sq cm/s.
    Keywords: SPACE RADIATION
    Type: NASA-CR-146333 , AD-A015673 , IGPP-UCR-75-16
    Format: application/pdf
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  • 9
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    Significance of medium energy gamma ray astronomy in the study of cosmic rays (1975)
    In:  CASI
    Details
    Publication Date: 2019-06-27
    Description: Medium energy (about 10 to 30 MeV) gamma ray astronomy provides information on the product of the galactic electron cosmic ray intensity and the galactic matter to which the electrons are dynamically coupled by the magnetic field. Because high energy (greater than 100 MeV) gamma ray astronomy provides analogous information for the nucleonic cosmic rays and the relevant matter, a comparison between high energy and medium energy gamma ray intensities provides a direct ratio of the cosmic ray electrons and nucleons throughout the galaxy. A calculation of gamma ray production by electron bremsstrahlung shows that: bremsstrahlung energy loss is probably not negligible over the lifetime of the electrons in the galaxy; and the approximate bremsstrahlung calculation often used previously overestimates the gamma ray intensity by about a factor of two. As a specific example, expected medium energy gamma ray intensities are calculated for the speral arm model.
    Keywords: SPACE RADIATION
    Type: NASA-TM-X-70988 , X-662-75-246
    Format: application/pdf
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  • 10
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    High energy gamma rays from Vela and Cygnus (1975)
    In:  Other Sources
    Details
    Publication Date: 2019-07-13
    Keywords: SPACE RADIATION
    Type: International Cosmic Ray Conference; Aug 15, 1975 - Aug 29, 1975; Munich
    Format: text
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