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  • Articles  (69)
  • Analytical Chemistry and Spectroscopy  (59)
  • Engineering General  (10)
  • Humans
  • 1980-1984
  • 1975-1979  (69)
  • 1975  (69)
  • 1
    Electronic Resource
    Electronic Resource
    The identification of 6-methoxy 8-aminoquionoline as a metabolite of primaquine in man (1975)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 2 (1975), S. 304-306 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The identification of 6-methoxy 8-aminoquinoline as a metabolite of Primaquine, an important antimalarial drug, is described. The metabolite is present in urine, plasma and erythrocytes following drug ingestion. It was identified by mass fragmentography of its 1H and 2H acetate and the acetate produced from authentic material. No evidence of further metabolites was obtained.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200020605
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  • 2
    Electronic Resource
    Electronic Resource
    Analysis of carotenoids by field desorption mass spectrometry (1975)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 10 (1975), S. 1102-1110 
    Details
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The mass spectra of a variety of authentic carotenoids covering a range of structural types have been studied using the field desorption technique. All the compounds examined show the molecular ion as the base peak, even where this ion is of very low intensity in the electron-impact spectra. Little fragmentation is observed, but thermal decomposition can be induced in certain cases by using higher emitter currents. Application to a simple mixture of authentic compounds and a more complex mixture of sedimentary origin shows the potential of the method in the rapid qualitative screening of carotenoids in crude extracts.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/oms.1210101207
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  • 3
    Electronic Resource
    Electronic Resource
    Nuclear magnetic resonance and the conformation of some derivatives of Michler's ketone (1975)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 7 (1975), S. 154-159 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: 1H NMR spectra are reported for Michler's ketone and twenty of its derivatives, along with 13C chemical shifts for five of the compounds. 1H chemical shifts show only small changes with increasing substitution at the sterically hindered 2-position. Estimates of the dihedral angle between the benzene ring and C—CO—C planes have been obtained from the chemical shifts of C=O and 4-C for ketones 1, 3, 5, 15 and 16. These angles are both internally consistent and very similar to dihedral angles determined by other methods for corresponding compounds in the benzophenone series.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270070403
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  • 4
    Electronic Resource
    Electronic Resource
    The atomic number dependence of the X-ray continuum intensity and the practical calculation of background in energy dispersive electron microprobe analysis (1975)
    New York, NY [u.a.] : Wiley-Blackwell
    X-Ray Spectrometry 4 (1975), S. 149-156 
    Details
    ISSN: 0049-8246
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: Computer fitting techniques have been used to derive a new expression for the relationship between X-ray continuum intensity and atomic number for a range of electron acelerating potentials up to 25 kV, continuum energies up to 10 keV and average atomic numbers up to thirty. A practical approach to background corrections in energy dispersive electron microprobe analysis, which utilizes this expression, is outlined. The procedure should lead to significant improvements in both accuracy and detection limits in this method of X-ray analysis.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/xrs.1300040311
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  • 5
    Electronic Resource
    Electronic Resource
    Cubic spline Galerkin approximations to parabolic systems with coupled non-linear boundary conditionsThis work was supported by the Rockwell International IR and D Interdivisional Technology Program under the sponsorship of the Mathematics and Statistics Technological Panel. (1975)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 9 (1975), S. 63-71 
    Details
    ISSN: 0029-5981
    Keywords: Engineering ; Engineering General
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: This paper describes a practical implementation of the Galerkin finite element procedure for solving systems of parabolic partial differential equations with non-linear boundary conditions. This technique consists of finding an approximation in the form of a finite sum of cubic B-splines, which yield high-order accurate results, and consequently, solutions can be developed with remarkable precision and speed up to the steady state region where conventional finite difference methods often fail. In addition, the choice of mesh width and nodal spacing can be automatically determined for a predictor-corrector routine, thereby relieving the engineer of a great deal of ‘guess work’ that is normally characteristic of solving such problems.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/nme.1620090106
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  • 6
    Electronic Resource
    Electronic Resource
    The direct numerical integration of linear matrix differential equations using pade approximations (1975)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 9 (1975), S. 259-270 
    Details
    ISSN: 0029-5981
    Keywords: Engineering ; Engineering General
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: A class of approximations to the matrix linear differential equation is presented. The approximations range, in accuracy, from the simplest forward difference scheme to the exact solution. The infinite series defining the exponential matrix is used to ascertain the accuracy of the various approximations. A clear distinction is made between approximations to the system equations and the forcing function, with the forcing term being represented by a piecewise linear function. Special application is given to the equations arising in structural dynamics of the form For these structural dynamic equations, the measure of the energy of the system is used to analyse the stability of the numerical approximations.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/nme.1620090202
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  • 7
    Electronic Resource
    Electronic Resource
    Three-dimensional elasto-plastic finite element analysis (1975)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 9 (1975), S. 209-218 
    Details
    ISSN: 0029-5981
    Keywords: Engineering ; Engineering General
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: Advances in technology and interest in limit state design have made the inclusion of non-linear effects, such as elasto-plastic behaviour, desirable in the analysis of many structures. Improvements in solution algorithms coupled with parallel developments in high speed digital computers have now made the practical solution of such problems possible. The paper presents numerical solutions to three-dimensional elasto-plastic problems illustrating the applicability of isoparametric elements and the order of computation times involved.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/nme.1620090115
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  • 8
    Electronic Resource
    Electronic Resource
    Finite element buckling analysis of homogeneous and sandwich plates (1975)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 9 (1975), S. 39-50 
    Details
    ISSN: 0029-5981
    Keywords: Engineering ; Engineering General
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: Finite element buckling analyses of plates are performed by means of quardrilateral elements having 12 degrees-of-freedom. It is found that if the plate is capable of appreciable transverse shear deformation, initial-stress stiffness matrices that represent the lateral dispalcement by cubic polynomials do not yield convergence to correct results. An initial-stress stiffness that works satisfactorily for both homogeneous and sandwich plates is formulated. A Fortran listing of the associated subroutine is provided.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/nme.1620090104
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  • 9
    Electronic Resource
    Electronic Resource
    Thermal deformation vector for a bilinear temperature distribution in an anisotropic quadrilateral membrane element (1975)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 9 (1975), S. 325-336 
    Details
    ISSN: 0029-5981
    Keywords: Engineering ; Engineering General
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: This paper presents a thermal-structural deformation vector for an anisotropic quadrilateral membrane element. The elastic properties of the element are based on linear stress assumptions and were developed by Robinson1. A general bilinear temperature field within the element is chosen in order to obtain a thermal deformation capability for the element commensurate with its elastic capability. A pseudo shear term is developed to account for part of the thermal deformation. The element is suitable for finite element analysis of advanced aircraft structures under elevated temperature environments and is particularly well suited for analysis of regions with severe temperature gradients such as occur in the vicinity of local heat sources and sinks. An example problem is included to demonstrate the behaviour of the element.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/nme.1620090205
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  • 10
    Electronic Resource
    Electronic Resource
    Uniform rational approximation of functions of several variables (1975)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 9 (1975), S. 297-323 
    Details
    ISSN: 0029-5981
    Keywords: Engineering ; Engineering General
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: We present a program which has given excellent results for uniform approximation of functions by polynomials, rational functions, generalized polynomials, and generalized rational functions. The algorithm is described in detail and several examples are discussed. The approximation is done over a finite point set, which is commonly a set of real numbers or points in the plane (in the latter case we are doing what is often known as surface fitting). Input to and output from the program is in tabular form. The method used is a linear programming approach known as the differential correction algorithm, which has been shown by several authors to always converge in theory (quadratically in some situations). In practice, we have obtained convergence in nearly every case, and quadratic convergence in most cases. The program can also be used for simultaneous approximation of several functions.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/nme.1620090204
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