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  • Physics  (2)
  • Wiley-Blackwell  (2)
  • American Institute of Physics
  • American Journal of Science
  • Copernicus
  • 1990-1994
  • 1970-1974  (2)
  • 1973  (2)
Collection
Keywords
Publisher
  • Wiley-Blackwell  (2)
  • American Institute of Physics
  • American Journal of Science
  • Copernicus
Years
  • 1990-1994
  • 1970-1974  (2)
Year
  • 1973  (2)
  • 1
    Electronic Resource
    Electronic Resource
    Small-angle x-ray scattering experiments for investigating the validity of the two-phase model (1973)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 11 (1973), S. 1219-1233 
    Details
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: A New method for evaluating SAXS curves of polymer samples with lamellar structure is applied to two typical scattering curves measured with a solution-crystallized linear polyethylene and a melt-crystallized branched polyethylene respectively. The method permits a rigorous check of the validity of the two-phase model and yields, without additional measurement, the volume fractions of the two phases and the difference in their densities. The densities can than be obtained by measuring the overall density of the sample. The results are: ρc = 0.996 g/cm3,ρa = 0.854 g/cm3, wa = 0.20 for the solution-crystallized sample; ρc = 0.967 g/cm3,ρa = 0.850 g/cm3, wa = 0.36 for the melt-crystallized sample.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1973.180110613
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  • 2
    Electronic Resource
    Electronic Resource
    α-Substituted diisopropylbenzene hydroperoxides for low-temperature SBR polymerizationPresented before the Rubber Division of the American Chemical Society, Boston, Massachusetts, April 25-28, 1972. (1973)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Chemistry Edition 11 (1973), S. 1589-1600 
    Details
    ISSN: 0360-6376
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Four pure hydroperoxides were evaluated as initiators for the polymerization of styrene-butadiene rubber (SBR) at 5°C. These materials were the meta and para isomers of mono- and dihydroperoxy-diisopropylbenzene. Results showed that the monohydroperoxides produced somewhat faster reactions than a control hydroperoxide, p-menthane hydroperoxide. Response to mercaptan level adjustments was good, providing polymer with a Mooney viscosity in the 50 to 60 range. The reaction rate with the dihydroperoxides was slower, but again provided polymer with a satisfactory viscosity. Basic physical property measurements on polymers prepared with the pure hydroperoxides or control hydroperoxides showed only minor differences. It is anticipated that these differences can be eliminated by small adjustments in the compound recipe.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1973.170110709
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