ISSN:
0018-019X
Keywords:
Chemistry
;
Organic Chemistry
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
Crystals of 1,6-cis-diaminocyclodecane dihydrochloride dihydrate are monoclinic, a = 8,145, b = 22,933, c = 9,393 A; β = 118° 20′; Z = 4; space group P21/c. The crystal structure has been determined by analysis of the three-dimensional PATTERSON function and refined by FOURIER and least squares methods using isotropic temperature factors. The conformation of the ring is the same as that observed for the trans-compound and the substituents occur on carbon atoms of type II, as predicted. The observed C—C—C angles are all larger than the tetrahedral angle, and range from about 113° to 120°.
Additional Material:
3 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/hlca.19610440729
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