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(E)-4-Bromo-2-[(2,6-diisopropylphenyl)iminomethyl]phenol (2012)

Balamurugan, P. ; Raja, K. Kanmani ; Rani, S. Kutti ; [et al.]

International Union of Crystallography

In: Acta Crystallographica Section E: Crystallographic Communications. 2012; 68(6): o1782-o1782. Published 2012 May 19. doi: 10.1107/s1600536812021605.

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Publication Date: 2012-05-19

Description: In the title compound, C19H22BrNO, the dihedral angle between the benzene rings is 76.17 (14)° and an intramolecular O—H...N hydrogen bond with an S(6) graph-set motif is present. One methyl group is disordered over two sets of sites with site occupancies of 0.66 (3) and 0.34 (3). A weak intermolecular C—H...π interaction is observed in the crystal structure.

Electronic ISSN: 1600-5368

Topics: Chemistry and Pharmacology , Geosciences

Published by International Union of Crystallography

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Crystal structure of 3,9,9-trimethyl-2,3,3a,4,9,9a-hexahydro-1H-cyclopenta[b]quinolin-4-ium chloride (2015)

Sridhar, G. ; Bilal, I. Mohammed ; Easwaramoorthy, D. ; [et al.]

International Union of Crystallography

In: Acta Crystallographica Section E: Crystallographic Communications. 2015; 71(7): o525-o526. Published 2015 Jun 27. doi: 10.1107/s2056989015011858.

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Publication Date: 2015-06-27

Description: The title molecular salt, C15H22N+·Cl−, arose as an unexpected product of the reaction between aniline and melanol in the presence of HCl. The central heterocyclic ring has a half-chair conformation and the five-membered ring has an envelope conformation, with the C atom linked to the N atom as the flap. In the crystal, the ions are linked by N—H...Cl hydrogen bonds, generating chains propagating in the [100] direction. The crystal studied was a merohedral twin with a 0.64 (3):0.36 (3) domain ratio.

Electronic ISSN: 2056-9890

Topics: Chemistry and Pharmacology , Geosciences

Published by International Union of Crystallography

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