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  • Articles  (9)
  • Articles: DFG German National Licenses  (9)
  • Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics  (9)
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  • Articles  (9)
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  • 1
    ISSN: 1573-4897
    Keywords: Flexural fatigue ; Glass reinforced composites
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Conclusions Flexural fatigue of uniaxially and biaxially stressed IPN/glass mat composites was investigated using four point bend (4PB) and concentrically loaded (CL) specimen geometries. Regions of nearly constant bending moment between the inner spans of a 4PB beam and within the inner annulus of a CL circular plate yield quasi-uniform uniaxial and biaxial stress, respectively, on the tensile faces. The specimen dimensions were optimized for both loading geometries to give: (1) reduced specimen deflection through maximizing the ratio of the induced tensile stresses to the applied load, (2) minimized contact stresses by maximizing the induced stress with respect to the unit contact load, and (3) a large material volume exposed to the maximum cyclic stress (i.e., statistical fracture initiation). A power model was used to analyze the fatigue data for the 4PB and CL specimens. Both IPN composite materials studied fatigued more rapidly under the more severe loading conditions imposed by the CL specimen geometry. Fractography revealed that debond fracture was the dominant damage process for both geometries. The initial debond cracks were uniformly distributed throughout the stressed regions, confirming the presence of nearly uniform tensile stress. Damage localization followed after further cycling and was characterized by a locally high debond fracture density, fiber fracture, and always occurred where several glass strands crossed near the specimen surface. Final specimen failure resulted from the preferential growth of dominant cracks through the specimen thickness.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 34 (1999), S. 5683-5687 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract In this work thermo-mechanical properties of MDF cements have been analyzed under complex thermal hystories. In particular the temperature sensitivity of the material has been investigated using dynamical-mechanical analysis. Several tests have been performed to investigate the behaviour of the material from room temperature to 250 °C at a fixed frequency (1 Hz). The viscoelastic behaviour of the composite was then analyzed at different frequencies: it was observed that the material exhibits two main transitions, around 60 °C and 160 °C. For comparison with differential scanning calorimeter analysis the first peak was attributed to the glass transition of the PVAAc while the second one was associated to the melting of the crystalline part of the polymer. In addition, dynamical-mechanical analysis that included complex thermal hystories, were performed both on pure polymer films, and on the MDF cements, confirming that the drop of mechanical properties with temperature is essentially due to the nature of the viscoelastic component. Results obtained are in agreement with the picture of a composite in which a polymeric thermoplastic matrix surrounds partially hydrated cement particles.
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  • 3
    ISSN: 1573-4811
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 34 (1999), S. 1899-1904 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract The structural relaxation process of an inorganic glass (Li2O2SiO2) at different cooling rates has been studied by differential scanning calorimetry. A four-parameter model – Tool-Narayanaswamy-Moynihan (TNM) model was applied to simulate the normalized specific heat curve measured. Four parameters, Δh*/R, β, ln A, and x were obtained and compared with the values obtained from the isothermal approach.
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  • 5
    Electronic Resource
    Electronic Resource
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 30 (1990), S. 314-320 
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Dynamic-mechanical and dielectric characterization of the cold crystallization of PEEK has been performed in order to develop a non-destructive evaluation method of crystallinity in thermoplastic matrices. The Avrami approach is applied here to describe the Poly(ether ether ketone) (PEEK) crystallization kinetics after an appropriate reduction of dynamic-mechanical and dielectric parameters. Avrami exponents obtained from dielectric characterization are comparable with those obtained with DSC measurements reported in literature, while the exponents obtained from the dynamic-mechanical characterization are higher, reflecting also changes in the aspect ratio of the growing crystals. Variations in the glass transition temperature detected during cold crystallization are analyzed and analogies between PEEK and PET are discussed.
    Additional Material: 9 Ill.
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  • 6
    Electronic Resource
    Electronic Resource
    Springer
    Mechanics of time-dependent materials 4 (2000), S. 139-154 
    ISSN: 1573-2738
    Keywords: composites ; fatigue ; graphite-epoxy ; stress ratio ; Weibull
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract A recent two-parameter fatigue model, aimed at the predictionof the fatigue behaviour of composite materials, was applied to fatigueresults available in the literature, concerning graphite/epoxy laminatessubjected to tension-compression loadings. It was found that the model,successfully applied in the case of tension-tension andcompression-compression fatigue, also works when the sign of stress isreversed during fatigue. However, the constants appearing in theproposed formula must be evaluated anew when the loading mode changesfrom pure tension to tension-compression. The probability of failure infatigue is predicted with reasonable accuracy by the model, which isvery conservative in calculating the residual strength after a givennumber of cycles.
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  • 7
    Electronic Resource
    Electronic Resource
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 28 (1988), S. 1203-1206 
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Thermal treatment of amorphous poly(aryl-ether-ether ketone) below the glass transition temperature has been studied. The extent of aging was measured by differential scanning calorimetry. X-ray and Fourier transform infrared spectra were used to study both melt-cast and annealed samples. The effect of the thermal treatment of viscoelastic response was evaluated using creep tests. Aging has been shown to be accompanied by a marked change in the transport properties of the material.
    Additional Material: 5 Ill.
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  • 8
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 39 (1990), S. 1163-1174 
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The viscoelastic properties of the amorphous and semicrystalline PEEK and of a PEEK-based composite (APC2) have been analyzed as a function of the aging time and related free volume relaxation, at temperatures close to the glass transition temperature. The effect of thermal treatments (physical aging) on the polymer amorphous phase of the three systems is presented. Creep tests approaching the “zero stress” were performed on samples subjected to different thermal histories. The presence of a second phase, namely crystallites and fibers, determines a loss of the mobility of the polymeric amorphous chains and consequently a decrease of the rate of free volume relaxation.
    Additional Material: 9 Ill.
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  • 9
    Electronic Resource
    Electronic Resource
    Brookfield, Conn. : Wiley-Blackwell
    Polymer Composites 14 (1993), S. 224-228 
    ISSN: 0272-8397
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The use of Wilhelmy plate techniques for studying the interactions of fibers with fluids of variable viscosity is discussed. The influence of hydrodynamic effects of force (F) VS. DEPTH (z) plots is interpreted on the basis of surface tension-independent added terms of the constitutive equation of the Wilhelmy experiment. Wetting experiments using pseudoplastic fluids (polyethyleneglycol/water solution) show that viscoelasticity is indeed important in the interpretation of Wilhelmy plate experiments. The comparison of wetting experiments performed on untreated and plasma-treated carbon fibers showed that at low stage speed and fluid viscosity, surface chemistry and morphology determines contact angles. At higher stage speeds and viscosities and advancing and receding angles are affected by surface chemistry-independent and hydrodynamics-dependent added contributions.
    Additional Material: 6 Ill.
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