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  • Wiley-Blackwell  (87)
  • 1
    Electronic Resource
    Electronic Resource
    Neue anorganische Ringsysteme. XX. Tricyclische anorganische Ringsysteme aus vier und fünf verschiedenen ElementenFrau Professor Margot Becke-Goehring zum 60. Geburtstage gewidmet (1974)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 406 (1974), S. 312-318 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Novel Inorganic Ring Systems. XX. Tricyclic Inorganic Ring Systems with Four and Five Different ElementsThe four ring systems D, E, F and G unknown solong, could be synthesized according to Schema 1. Their structure was confirmed by mass, proton resonance, and infrared spectroscopy. The single compounds are characterized by a deep green colour and an unusually high solubility in indifferent organic solvents.
    Notes: Die vier bisher unbekannten Ringsysteme D, E, F und G konnten nach den Angaben des Schema 1 synthetisiert werden. Ihre Struktur wurde durch Massen-, NMR- und IR-Spektren sowie Röntgenstrukturanalysen sichergestellt. Die einzelnen Verbindungen zeichnen sich durch eine tiefgrüne Farbe und ungewöhnlich hohe Löslichkeit in inerten organischen Lösungsmitteln aus.
    Additional Material: 5 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19744060226
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  • 2
    Electronic Resource
    Electronic Resource
    Komplexe aus Molybdänoxidtrichlorid und Aminosäure-Derivaten (1975)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 417 (1975), S. 41-46 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Coordination Compounds from Molybdenum Oxide Trichloride and Amino-acid DerivativesFormation of complexes of type B (look Scheme 1) between MoOCl3 and aminoacid derivatives occurs according to eq. 1-4 by reaction of MoOCl5 in methanol, ethanol or diethyl ether as well as by direct reaction of MoOCl3 with the ligands. They were confirmed in their constitution by analysis, magnetic investigations, mass, infrared and electron spectra, but not determined in their steric conformation.
    Notes: MoCl5 bildet mit Aminosäurederivaten in Methanol, Äthanol oder Diäthyläther gemäß Rkk. 1-3 grünkristalline MoOCl3-Aminosäurederivat-Komplexe des Typs B(s. Schema 1), die auch direkt aus den Komponenten entstehen (Rk. 4). Sie wurden durch Analysen, magnetische Messungen, Massen-, IR- und Elektronenspektren in ihrer Konstitution festgelegt nicht aber in ihrer sterischen Konformation aufgeklärt.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19754170107
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  • 3
    Electronic Resource
    Electronic Resource
    Beiträge zur Chemie der Silicium-Stickstoff-Verbindungen. CXXXI. 1,2-Bis(organy lamino)-tetramethyldisilane und ihre Überführung in N,N′-Bis(organyl)oktamethyl-tetrasiladiazacyclohexane (1976)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 419 (1976), S. 41-47 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Chemistry of Silicon-Nitrogen Compounds. CXXXI. 1,2-Bis (organylamino) - tetramethyldisilaries and their Transformation into N,N′-Bis (organyl) octamethyltetrasiladiaza-cyclohexanes1,2-Bis(organylamino)disilanes A 1-4 were prepared via equ. 3 by aminolysis of 1,2-dichlorotetramethyldisilane and transformed by three different methods (equ. 7; 8/9 and 10/11) into the N,N′ variied tetrasiladiazacyclohexanes B 2-5. Physical, analytical and structural information can be taken from tables 1-3. The bond increments (N)Si—Si(N) of the EISENLOHR molar refractions MRE were reinvestigated with 24.5 instead of 30.0.
    Notes: Organylaminolyse des 1,2-Dichlortetramethyldisilans führt nach Rk. 3 zu den entsprechenden 1,2-Bis(organylamino)-Derivaten A 1-4. Sie ließen sich auf 3 verschiedenen Wegen (Rkk, 7, 8/9 bzw. 10/11) in die N,N′-variierten Tetrasiladiazacyclohexane B 2-5 überführen. Physikalische, analytische und strukturelle Daten der neu dargestellten Verbindungen finden sich in Tab. 1-3. Das Bindungsinkrement (N)Si-Si(N) für die Molrefraktionen MRE nach EISENLOHR wurde neu bestimmt zu 24,5, bisher 30,0.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19764190108
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  • 4
    Electronic Resource
    Electronic Resource
    Beiträge zur Chemie der Silicium-Stickstoff-Verbindungen. CXXXII. Derivate des 1,2,3-Trisila-3,5-diaza-cyclopentan-Ringsystems (1976)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 419 (1976), S. 48-57 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Chemistry of Silicon-Nitrogen Compounds. CXXXII. Derivatives of the 1,2,4-Trisila-3,5-diaza-cyclopentane Ring SystemThe derivatives B1-B6 of the title ring system could be prepared for the first time by reaction of 1,2-bis(alkylamino)disilanes (A1, A2) with dihalosilanes (Scheme 1). They were transformed by additional reactions with methanol or amines into B7-B9. The Cl2Si derivative B2 is characterized by an unusual stability against aqueous solutions.
    Notes: Durch Reaktion von Dihalogensilanen mit 1,2-Bis(alkylamino)disilanen (A1, A2) konnten die Derivate B1-B6 des Titelringsystems und durch deren weitere Umsetzung die Verbindungen B7-B9 erstmalig dargestellt werden (Schema 1). B2 zeichnet sich durch eine ungewöhnliche Stabilität gegenüber neutralen wäßrigen Lösungen aus.
    Additional Material: 4 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19764190109
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  • 5
    Electronic Resource
    Electronic Resource
    Neue anorganische Ringsysteme. XXII. Neue Spirosilazane der Gerüsttypen Si5N4, Si5N5, Si5N4O und Si7N8 (1976)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 419 (1976), S. 108-114 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Novel Inorganic Ring Systems. XXII. Novel Spirosilazanes of the Si5N4, Si5N5, Si5N4O, and Si7N8 SkeletonWe succeeded in preparing the four novel spirosilazane skeletons E, F, G, and H of the composition given in the title. The permethylated compounds of the mentioned systems have been characterized in their chemical and physical properties. The conformation of their structure was possible by elemental analysis and by n.m.r., mass, i.r., and Raman spectra.
    Notes: Es gelang, die vier neuen Spirosilazangerüste E, F, G und H der im Titel angegebenen Gerüsttypen in den jeweils permethylierten Vertretern über die Reaktionen 1-5 zu synthetisieren und in ihren chemischen und physikalischen Eigenschaften zu charakterisieren. Die Strukturaufklärung erfolgte über Elementaranalysen, 1H-NMR-, Massen-, IR- und Raman-Spektren.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19764190203
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  • 6
    Electronic Resource
    Electronic Resource
    Neue anorganische Ringsysteme. XXIII. Hetero-Spirosilazane mit Germanium, Zinn und Zirkonium als spiralem Zentrum (1976)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 419 (1976), S. 115-120 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Novel Inorganic Ring Systems. XXIII. Hetero Spirosilazanes with Ge, Sn, and Zr in the Spiral CenterSymmetrical SiN-spiro[4,4]-nonanes of the skeleton composition Si5N4, Si4N4Ge, Si4N4Sn and Si4N4Zr and with the hetero atoms in the spiral center could be prepared for the first time in shape of their permethylated derivatives A1 to E1 via equations (1/2) as well as (3/4/5/6) respectively. They were confirmed in their structure by elemental analysis, proton n.m.r., mass, i.r., and Raman spectra.
    Notes: Symmetrische Silaza-spiro[4,4]-nonane der Gerüsttypen Si5N4, Si4N4Ge, Si4N4Sn und Si4N4Zr und mit den Heteroatomen als spiralen Zentren konnten in Form ihrer permethylierten Derivate A1 bis E1 über die Reaktionswege (1/2) bzw. (3/4/5/6) erstmalig dargestellt und in ihrer Struktur über Elementaranalyse, 1H-NMR, Massen-, IR- und Raman-Spektren eindeutig bestätigt werden.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19764190204
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  • 7
    Electronic Resource
    Electronic Resource
    Neue anorganische Ringsysteme. XXVII [1, 2]. Die Ringsysteme des Arsa- und des Stibia-disila-diaza-cyclopentans (1976)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 424 (1976), S. 87-92 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Novel Inorganic Ring Systems. XXVII. The Ring Systems of Arsa- and Stibia-disila-diaza-cyclopentane1.2-Bis(alkylamino)disilanes react with AsCl3 and SbCl3 respectively to give the novel five membered ring systems B and C. AsCl units in B 1-3 can be substituted leading to B 4-6. The properties of the new compounds are described. Their structure was confirmed by elemental analysis, mass, proton n.m.r., and infrared spectroscopy.
    Notes: 1.2-Bis(alkylamino)disilane setzen sich mit AsCl3 bzw. SbCl3 zu den neuen fünfgliedrigen Ringsystemen B bzw. C um. AsCl-Einheiten in B 1-3 lassen sich zu B 4-6 substituieren. Die Eigenschaften der neuen Verbindungen werden beschrieben. Ihre Strukturbestimmung erfolgte über Elementaranalysen, Massen-, Protonenresonanz- und Infrarot-Spektren.
    Additional Material: 4 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19764240113
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  • 8
    Electronic Resource
    Electronic Resource
    Neue anorganische Ringsysteme. 28. Das Spiro[4,3]-tetrasilatetrazaoktan-System (1977)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 429 (1977), S. 74-82 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Novel Inorganic Ring Systems. 28. The Spiro[4,3]-tetrasilatetrazaoctane SystemAccording to scheme 3 the spiro[4,3]-tetrasilatetrazaoctanes B are formed with high yields. Their properties are described. Physical and analytical data as well as some results for the proof of structure can be taken from tables 1—3. The very easy proceeding hydrolysis of B2 leads to A8 (scheme 4). On the contrary hydrolysis of A1 is difficult to realize and results in A3 as the main product (scheme 2).
    Notes: Nach Schema 3 bilden sich mit hohen Ausbeuten die Spiro[4,3]-tetrasilatetrazaoktane B1-5. Ihre Eigenschaften werden beschrieben. Physikalische, elementar- und strukturanalytische Daten sind in den Tab. 1-3 niedergelegt. Die sehr leicht ablaufende Hydrolyse von B2 führt zu A8 (Schema 4), die nur sehr schwer zu realisierende von A1 ergibt als Hauptprodukt A3 (Schema 2).
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19774290110
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  • 9
    Electronic Resource
    Electronic Resource
    Beiträge zur Chemie der Silicium-Stickstoff-Verbindungen. 140. Das anorganische Fünfringsystem des Cyclobordisildiazans (1977)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 429 (1977), S. 83-87 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Contributions to the Chemistry of Silicon-Nitrogen Compounds. 140. The Inorganic Fivemembered Ringsystem of Cyclobordisildiazane1,2-Bis(alkylamino)disilanes react with dichloroboranes, Cl2BR, according to eq. (2) to give the derivatives A2—A11 of the fivemembered cyclobordisildiazane system. The properties of the new compounds are described. Their structure was confirmed by elemental analysis, mass, proton nmr, and infrared spectroscopy.
    Notes: 1,2-Bis(alkylamino)disilane setzen sich mit Dichlorboranen, Cl2BR, gemäß Rk. (2) zu den Derivaten A2-A11 des Cyclobordisildiazan-Fünfringsystems um. Die Eigenschaften der neuen Verbindungen werden beschrieben. Ihre Strukturbestimmung erfolgte über Elementaranalysen, Massen-, Protonenresonanz- und Infrarot-Spektren.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19774290111
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  • 10
    Electronic Resource
    Electronic Resource
    Neue anorganische Ringsysteme, 30 [1, 2]. Cyclo-germadisiladiazane (1978)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 439 (1978), S. 83-89 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Novel Inorganic Ring Systems. 30. Cyclo-germadisiladiazanesThe Fivemembered ring system of a germadisiladiazane was prepared for the first time according to scheme 1. Compounds A 1, 8,13 could be transformed into their derivatives A 2-7 and 9-12 (scheme 2). The properties of the new compounds are described (Table 2). Proof of their constitution is given by elemental analysis, mass, proton n.m.r., and infrared spectra (Tables 3-6).
    Notes: Das Fünfringsystem des Germadisiladiazans wurde erstmalig gemäß Schema 1 in den Verbindungen A 1, 8, 13 dargestellt. Diese ließen sich zu den Derivaten A 2-7 und 9-12 weiter umsetzen (Schema 2). Alle Verbindungen werden in ihren Eigenschaften beschrieben (Tab. 2). Ihre Konstitution geht aus Elementaranalysen (Tab. 3), Massen-, 1H-NMR- und IR-Spektren eindeutig hervor (tab. 4-6).
    Additional Material: 6 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19784390109
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