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Structure of chlorinated poly(vinyl chloride). X. Conclusions on the chlorination mechanism (1981)

Lukáš, R. ; Světlý, J. ; Kolínský, M.

New York : Wiley-Blackwell

Journal of Polymer Science: Polymer Chemistry Edition 19 (1981), S. 295-304

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ISSN: 0360-6376

Keywords: Physics ; Polymer and Materials Science

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The chlorination of poly(vinyl chloride) (PVC) was investigated by using deuterated polymeric models of PVC, viz., α-deuterated PVC (α-d-PVC) and β,β-dideuterated PVC (β,β-d2-PVC). The chlorinated samples of PVC, α-d-PVC, and β,β-d2-PVC were examined by combining infrared (IR), 1H-NMR, 13C-NMR, and mass spectroscopy. The results obtained were used in a study of the reaction mechanism of PVC chlorination. The selectivity of chlorination and the extent of the substitution and elimination-addition mechanism of chlorination are discussed with respect to the degree of chlorination and chlorination conditions.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/pol.1981.170190207

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