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  • 1
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    American Association for the Advancement of Science (AAAS)
    Publication Date: 1981-03-13
    Description: Great advances have been made in fundamental scientific research in recent years. The new knowledge gathered, in addition to deepening our understanding of the physical universe, contributes a range of abilities and opportunities to society that would not otherwise be available. Much research that may be called applied because it addresses needs of society is quite fundamental in character, and support of such research at the National Science Foundation is to be handled in tandem by the research directorates. Other areas that require a refocusing of support are engineering science and education, at all levels, in science and engineering. Increasing our strength in these areas is essential to achieve our national economic, social, and political goals. Steps are being taken by the National Science Foundation to make its structure better able to deal with engineering and applied research and to provide greater mutual reinforcement between applied and basic research.〈br /〉〈span class="detail_caption"〉Notes: 〈/span〉Slaughter, J B -- New York, N.Y. -- Science. 1981 Mar 13;211(4487):1131-6.〈br /〉〈span class="detail_caption"〉Record origin:〈/span〉 〈a href="http://www.ncbi.nlm.nih.gov/pubmed/7466384" target="_blank"〉PubMed〈/a〉
    Keywords: Cell Biology ; Chemical Phenomena ; Chemistry ; *Forecasting ; Geological Phenomena ; Geology ; *Government Agencies ; Molecular Biology ; Neurochemistry ; Physical Phenomena ; Physics ; Research Support as Topic ; United States
    Print ISSN: 0036-8075
    Electronic ISSN: 1095-9203
    Topics: Biology , Chemistry and Pharmacology , Computer Science , Medicine , Natural Sciences in General , Physics
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  • 2
    Unknown
    Amsterdam ; New York : North-Holland Pub. Co
    Keywords: DDC 530.1 ; LC QC20 ; Mathematical physics ; Physics ; Quantum theory ; Relativity (Physics)
    ISBN: 9780444875853
    Language: English
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  • 3
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 18 (1980), S. 1237-1242 
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Electron microscopy reveals a high-temperature morphological transition in a styrene-butadiene-styrene block copolymer of 7000 polystyrene block molecular weight and 43,000 polybutadiene block molecular weight (7S-43B-7S). Samples quenched in liquid nitrogen from temperatures above 150°C show no structure, whereas those quenched from temperatures below 140°C clearly show a multiphase structure. We previously reported that the 7S-43B-7S polymer exhibits a relatively sharp melt rheological transition in the temperature region between 140 and 150°C from highly viscoelastic and nonlinear viscous behavior to linear viscous behavior with insignificant elasticity. The dynamic viscoelastic properties are measured at different strain amplitudes in this study, and the results show that the melt rheological transition behavior is not influenced by the strain amplitude. This study clearly shows that the melt rheological transition in the 7S-43B-7S results from a morphological transition from a multiphase structure below about 140°C to a single-phase structure above about 150°C.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 18 (1980), S. 1257-1270 
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: The intensity of the glass transition in semicrystalline polycarbonate was measured by differential scanning calorimetry and by thermally stimulated discharge of electrets. Solution-cast and bulk-crystallized samples possessing widely varying crystallinities and morphologies were investigated. It is shown that the intensity of the glass transition is governed by the extent of primary crystallization and is a linear combination of intensities from the bulk amorphous regions and from noncrystalline polymer within semicrystalline aggregates such as spherulites. The intensity of the glass transition within spherulites is about 0.1-0.3 as great as that in bulk amorphous regions. A three-phase model incorporating two distinct types of noncrystalline polycarbonate is proposed to account for the properties of this polymer.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 18 (1980), S. 1311-1324 
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: A detailed description of the morphology and the complex melting behavior of poly(ethylene terephthalate) crystallized isothermally in the range 100-245°C is presented. Double or single melting endotherms can deliberately be obtained by varying the heating rate in the differential scanning calorimeter (DSC). In the case of double melting peaks, the first endotherm (I) corresponds to the melting of the crystalline material formed at the crystallization temperature Tc. The second melting endotherm (II) originates from the melting of a fraction of the original crystalline material reorganized during the DSC scan. The appearance of one melting endotherm (I or II) relates to the melting of the original structure or the melting of a completely transformed structure. Taking the end of the melting endotherm I as the final melting temperature TM of the material, an equilibrium melting temperature of 290°C is obtained from a plot of TM vs. Tc. A detailed morphological study of the isothermally crystallized samples by electron microscopy and both small-angle and wide-angle x-ray scattering raises questions about the use of the two-phase concept in relating morphological parameters and melting behavior at low crystallization temperatures.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 18 (1980), S. 1361-1381 
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: A temperature-dependent small-angle x-ray scattering and electron microscopic study on a sample of low-density polyethylene affords a determination of the structure changes in a heating and cooling cycle and suggests a new model of partial crystallization and melting. The analysis of SAXS data is based upon some general properties of the electron-density correlation function. Electron micrographs are obtained from stained sections γ irradiated at elevated temperatures and are analyzed quantitatively by statistical means. According to the model proposed here the thickness distribution in the amorphous layers, rather than that of the crystalline regions, is the essential factor governing the crystallization and melting behavior. The temperature-dependent changes in this thickness distribution provide a natural explanation for the large reversible changes in long-spacing.
    Additional Material: 16 Ill.
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 18 (1980), S. 1421-1431 
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Solid solutions of two low-molecular-weight polyethylene fractions, formed by rapid quenching from the melt, were studied by differential scanning calorimetry, low-frequency Raman spectroscopy, and Fourier-transform infrared spectroscopy. Two kinds of defects exist in these solid solutions; namely, a disruption of chain extension and the presence of monoclinic packing. The distribution of fully extended chain-segment lengths and the intensity of the 717 cm-1 infrared band, characteristic of the monoclinic phase, are found to be composition dependent. Our spectroscopic studies of the solid solutions support the model first proposed by Ott and Slagle.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 18 (1980), S. 1413-1419 
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: The thermal behavior of α nylon-12 film cast from a phenol-ethanol mixture has been studied by differential scanning calorimetry. Polymorphism has been analyzed by x-ray diffraction. The γ form exhibits a single endothermic melting peak in the thermogram, whereas the α form exhibits double peaks. Samples with mixed α and γ forms show double peaks at the same positions and the area ratio changes in accordance with the amounts of the two forms. The appearance of the γ peak, even for the α sample, is explained by recrystallization to the γ form after melting of the α form. The melting point of α nylon-12 is ca. 173°C, which is lower by 6-7° than that of the γ form. Once the α or γ sample has been melted and then cooled, its heating thermogram shows a small peak before the appearance of the main peak. The small peak seems to be due to incomplete and/or smaller crystallites formed during cooling. Heat treatment below the melting point of α nylon-12 is effective in transforming the α form to the γ form, probably via a melt-recrystallization process.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 18 (1980), S. 1433-1438 
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: A 40:60 mole ratio poly(ethylene terephthalate-co-p-oxybenzoate) was studied by dynamic scanning calorimetry. Vitrification occurred in two steps, which could be linked by optical microscopy to a two-phase structure. For the lower glass transition, hysteresis was absent on heating and cooling through the transition temperature. Since all prior studied glasses show such hysteresis, this may be linked to the mesophase structure and raises the question whether mesophases always display such glass-transition behavior.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 18 (1980), S. 1469-1480 
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: A small-angle x-ray scattering (SAXS) investigation of two linear segmented polyurethanes was carried out to learn about the respective domain structure (morphology). Both urethanes had a hard segment of methylene-bis(4)phenyl isocyanate (MDI) and butanediol. These two components comprised 28% by weight of each system. The soft segments differed in that one was a polyether (tetramethylene oxide, molecular weight 1000), while the other was a polyester (polytetramethylene adipate, molecular weight 1000). Both of these segmented urethanes were stored at room temperature for over 6 months prior to investigation. Using an automated Kratky camera, SAXS scans were made. By detailed analysis (using the computer program of Vonk) the average interfacial thickness E of the domains was determined by two approaches. The value of E for the polyester was 10-12 Å, while it was 5-7 Å for the polyether. Within the limits of the assumptions used for analysis, these data directly support the conjecture that polyether urethanes generally lead to better phase separation. Other aspects of the analysis provided further information on the morphological structure. Some cautionary comments are provided on the use of quantitative SAXS data obtained from these or similar systems.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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