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  • 05. General::05.09. Miscellaneous::05.09.99. General or miscellaneous
  • Dielectric properties
  • Instrumentation
  • American Chemical Society  (2)
  • Springer Netherlands  (2)
  • American Institute of Physics (AIP)
  • 1
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    Blackening of Pompeian Cinnabar paintings: X-ray micro-spectroscopy analysis (2007)
    American Chemical Society
    Details
    Publication Date: 2017-04-04
    Description: Red Pompeian paintings, very famous for their deep intensity, are currently suffering from darkening. The origins of this darkening degradation are not clearly identified yet and remain a major issue for curators. In the specific case of cinnabar (HgS)-based red pigment, a photoinduced conversion into black metacinnabar is usually suspected. This work is focused on the blackening of red cinnabar paintings coated on a sparry calcite mortar. Different samples exhibiting different levels of degradation were selected upon visual observations and analyzed by synchrotron-based microanalytical techniques. Atomic and molecular compositions of the different debased regions revealed two possible degradation mechanisms. On one hand, micro X-ray fluorescence elemental maps show peculiar distributions of chlorine and sulfur. On the other hand, X-ray absorption spectroscopy performed at both Cl and S K-edges confirms the presence of characteristic degradation products: (i) Hg- Cl compounds (e.g., corderoite, calomel, and terlinguaite), which may result from the reaction with exogenous NaCl, in gray areas; (ii) gypsum, produced by the calcite sulfation, in black coatings. Metacinnabar is never detected. Finally, a cross section was analyzed to map the in-depth alteration gradient. Reduced and oxidized sulfur distributions reveal that the sulfated black coating consists of a 5-ím-thick layer covering intact cinnabar.
    Description: Published
    Description: 7484-7492
    Description: reserved
    Keywords: Microspectroscopy Analysis ; 05. General::05.09. Miscellaneous::05.09.99. General or miscellaneous
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 2
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    Influence of instruments on the H/V spectral ratios of ambient vibrations (2007)
    Springer Netherlands
    Details
    Publication Date: 2017-04-04
    Description: For an optimal analysis of the H/V curve, it appears necessary to check the instrument signal to noise ratio in the studied frequency band, to ensure that the signal from the ground noise is well above the internal noise. We assess the reliability and accuracy of various digitizers, sensors and/or digitizer-sensor couples. Although this study is of general interest for any kind of seismological study, we emphasize the influence of equipment on H/V analysis results. To display the impact of the instrumental part on the H/V behavior, some series of tests have been carried out following a step-by-step procedure: first, the digitizers have been tested in the lab (sensitivity, internal noise...), then the three components sensors, still in the lab, and finally the usual user digitizers-sensors couple in lab and outdoors. In general, the digitizer characteristics, verified during this test, correspond well to the manufacturer specifications, however, depending on the digitizer, the quality of the digitized waveform can be very good to very poor, with variation from a channel to another channel (gain, time difference etc.). It appears very clearly that digitizers need a warming up time before the recording to avoid problems in the low-frequency range. Regarding the sensors, we recommend strongly to avoid the use of “classical” accelerometers (i.e., usual force balance technology). The majority of tested seismometers (broadband and short period, even 4.5 Hz) can be used without problems from 0.4 to 25 Hz. In all cases, the instrumentation should be checked first to verify that it works well for the defined study aim, but also to define its limit of use (frequency, sensitivity...).
    Description: Published
    Description: 3-31
    Description: 4.1. Metodologie sismologiche per l'ingegneria sismica
    Description: JCR Journal
    Description: reserved
    Keywords: H/V technique ; Instrumentation ; Microtremors ; Site effects ; 04. Solid Earth::04.06. Seismology::04.06.99. General or miscellaneous ; 04. Solid Earth::04.06. Seismology::04.06.10. Instruments and techniques
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 3
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    Modeling the 2004 Sumatra tsunami at Seychelles Islands: site-effect analysis and comparison with observations (2014)
    Springer Netherlands | Springer Science+Business Media B.V.
    Details
    Publication Date: 2017-04-04
    Description: The Mw = 9.1 mega-thrust Sumatra–Andaman earthquake that occurred on December 26, 2004, was followed by a devastating tsunami that killed hundreds of thousands of people and caused catastrophic effects on human settlements and environments along many coasts of the Indian Ocean, where even countries very far from the source were affected. One of these cases is represented by the Republic of Seychelles, where the tsunami reached the region about 7 h after the earthquake and produced relevant damages, despite the country was more than 4,500 km far from the seismic source. In the present work, we present and discuss a study of the 2004 Sumatra tsunami by means of numerical simulations with the attention focused on the effects observed at the Seychelles Archipelago, a region never previously investigated with this approach. The case is interesting since these islands lay on a very shallow oceanic platform with steep slopes so as the ocean depth changes from thousands to few tens of meters over short distances, with significant effects on the tsunami propagation features: the waves are strongly refracted by the oceanic platform and the tsunami signal is modified by the introduction of additional frequencies. The study is used also to validate the UBO-TSUFD numerical code on a real tsunami event in the far field, and the results are compared with the available observations, i.e., the sea level time series recorded at the Pointe La Rue station, Mahe ́ Island, and run-up measurements and inundation lines surveyed few weeks after the tsunami at Praslin Island, where the tsunami hit during low tide. Synthetic results are found in good agreement with observations, even though some of the observations remain not fully solved. Moreover, simulations have been run in high-tide condition since the 2004 Sumatra tsunami hitting at high tide can be taken as the worst-case scenario for the Seychelles islands and used for tsunami hazard and risk assessments
    Description: Published
    Description: 1507–1525
    Description: 4T. Fisica dei terremoti e scenari cosismici
    Description: JCR Journal
    Description: restricted
    Keywords: Tsunami; Numerical modeling; Indian Ocean; Tsunami scenarios ; 05. General::05.09. Miscellaneous::05.09.99. General or miscellaneous
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 4
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    Flow-through quantification of microplastics using impedance spectroscopy (2021)
    American Chemical Society
    Details
    Publication Date: 2022-10-21
    Description: © The Author(s), 2021. This article is distributed under the terms of the Creative Commons Attribution License. The definitive version was published in Colson, B. C., & Michel, A. P. M. Flow-through quantification of microplastics using impedance spectroscopy. ACS Sensors, 6(1), (2021): 238–244, doi:10.1021/acssensors.0c02223.
    Description: Understanding the sources, impacts, and fate of microplastics in the environment is critical for assessing the potential risks of these anthropogenic particles. However, our ability to quantify and identify microplastics in aquatic ecosystems is limited by the lack of rapid techniques that do not require visual sorting or preprocessing. Here, we demonstrate the use of impedance spectroscopy for high-throughput flow-through microplastic quantification, with the goal of rapid measurement of microplastic concentration and size. Impedance spectroscopy characterizes the electrical properties of individual particles directly in the flow of water, allowing for simultaneous sizing and material identification. To demonstrate the technique, spike and recovery experiments were conducted in tap water with 212–1000 μm polyethylene beads in six size ranges and a variety of similarly sized biological materials. Microplastics were reliably detected, sized, and differentiated from biological materials via their electrical properties at an average flow rate of 103 ± 8 mL/min. The recovery rate was ≥90% for microplastics in the 300–1000 μm size range, and the false positive rate for the misidentification of the biological material as plastic was 1%. Impedance spectroscopy allowed for the identification of microplastics directly in water without visual sorting or filtration, demonstrating its use for flow-through sensing.
    Description: The authors thank the Richard Saltonstall Charitable Foundation and the National Academies Keck Futures Initiative (NAKFI DBS13) for their funding support.
    Keywords: Microplastics ; Plastics ; Impedance spectroscopy ; Dielectric properties ; Instrumentation ; Particle detection ; Flow-through ; Environmental sensing
    Repository Name: Woods Hole Open Access Server
    Type: Article
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