Digitale Medien
Copenhagen
:
International Union of Crystallography (IUCr)
Applied crystallography online
1 (1968), S. 61-67
ISSN:
1600-5767
Quelle:
Crystallography Journals Online : IUCR Backfile Archive 1948-2001
Thema:
Geologie und Paläontologie
,
Physik
Notizen:
The long range order in a powder sample of Ag3Mg has been studied by X-ray diffraction as a function of quenching temperature below the critical ordering temperature of 665°K. By measuring the positions and integrated intensities of fundamental, superlattice and satellite reflections, the latter arising from the periodic anti-phase boundary structure, the variation with temperature of the overall long range order, antiphase boundary order, and anti-phase boundary periodicity have been determined. It appears that the anti-phase boundaries disorder slightly more with increasing temperature than the average superlattice, and that the boundary spacing, nominally equal to two (M = 2), increases towards that ideal value with increasing disorder below the critical point. These resalts are qualitatively interpreted by extending the reasoning of Sato & Toth on equilibrium long period superlattices to include the case where the Fermi surface becomes progressively more diffuse with increasing disorder.
Materialart:
Digitale Medien
URL:
http://dx.doi.org/10.1107/S0021889868005017
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