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  • Springer  (57,589)
  • American Physical Society  (8,822)
  • American Physical Society (APS)
  • International Union of Crystallography (IUCr)
  • 1985-1989  (67,639)
  • 1989  (67,639)
  • 1
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 182-183 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Easy and convenient techniques have been developed to handle air-sensitive compounds in terms of measuring their single-crystal X-ray diffraction intensities. These methods have also been fruitfully applied in collecting X-ray data of several highly air-sensitive inorganic and organometallic compounds without using a cold stream of nitrogen.
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  • 2
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 187-187 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 209-215 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Point-defect aggregates in (111) dislocation-free silicon single crystals grown by the float-zone (FZ) method have been studied by diffuse X-ray scattering (DXS) and compared with those in the Czochralski-grown (CZ) crystals. A two-axis X-ray diffractometer was used. It employs three monochromators in (+, −, −) setting to obtain a highly collimated and monochromatic Mo Kα1 beam. DXS measurements were made around the 111 reciprocal-lattice point (r.l.p.) with K* along ±[111] and ±[01{\bar 1}]; K is the vector which joins the elemental volume of the reciprocal space under investigation to the nearest r.l.p. For FZ crystals for a given K* the DXS intensity was higher for θ 〈 θB in comparison with that for θ 〉 θB showing that the anisotropy (DXS Iθ 〉 θB − DXS Iθ 〈 θB) is negative, as expected for vacancy clusters. For CZ crystals the anisotropy was positive, owing to the presence of interstitial clusters. The magnitude of anisotropy in the FZ crystals was smaller than that observed in the CZ crystals. The DXS intensity varies approximately as K−2 near Bragg peaks (Huang scattering) and as K*−4 (Stokes–Wilson scattering) away from it. From the K* values where the changeover from Huang to Stokes–Wilson scattering takes place the size of the clusters assumed to be the origin of the observed DXS is estimated as ̃2 × 10−4 and 2.6 × 10−3 mm for FZ and ̃5.5 × 10−4 and 3 × 10−3 mm for CZ crystals. The experimental data were compared with theoretically calculated DXS distributions assuming the defects to be dislocation loops. The number of point defects in a loop has been estimated.
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  • 4
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 205-208 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: The effect of texture on the interpretation of the classical radial distribution function (RDF) is studied. A model of axial texture is presented which enables the calculation of the effect for individual interatomic distances and an analysis of the effect on the global RDF. The example shows that the shift of the RDF closest-neighbour peak position can be as large as 0.06 Å.
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  • 5
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 216-221 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: The components of a symmetric second-rank tensor (e.g. the strain tensor) can be calculated from measurements of that tensor property in at least six directions. A system of simultaneous equations (t(m) = Σ6i = 1 amiti) must be solved. The coefficient matrix ami is determined by the measurement directions, and therefore it is of great importance to choose these directions properly. Part 1 deals with the necessary condition: rank (ami)〈〉 0. Rules are given by which it is easy to decide whether rank (ami) = 0 or rank (ami) ≷0 without calculating the rank. In part 2 methods are developed to find optimized sets of measurement directions. An optimized set is one for which the inevitable measurement errors will give errors of the calculated tensor components as small as possible. Special attention is given to the case of X-ray strain measurement of single crystals.
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  • 6
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 308-314 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Following the discovery of systems with diffraction patterns exhibiting icosahedral symmetry by Shechtman, Blecht, Gratias & Cahn [Phys. Rev. Lett. (1984), 53, 1951–1953], which is forbidden in classical crystallography, interest has centred on Penrose tiling and its generalizations as a model for the explanation of these patterns, although Pauling [Nature (London) (1985), 317, 512–514; Phys. Rev. Lett. (1987), 58, 365–368] has proposed an alternative explanation in terms of crystal twinning. In an attempt to reconcile these two points of view a computer algorithm has been developed, following the methods outlined by Wolny, Pytlik & Lebech [J. Phys. C (1988), 21, 2267–2277], to grow a number of different structures which all tile the two-dimensional (2D) plane without defects. With the same two types of basic unit, it is shown that it is possible, on the one hand, to produce structures similar to the Penrose tiling pattern and, on the other, different types of twinned and disordered structures, with a continuous sequence of intermediates. Optical diffraction patterns of these structures have been obtained for comparison with real quasi-crystals.
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  • 7
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 380-380 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Owing to a printer's error, the fourth equation given in the Abstract of the paper by Åsbrink, Kihlborg & Malinowski [J. Appl. Cryst. (1988). 21, 960–962] is incorrect. The correct equation is {\bar \beta}_c(0–7.41 GPa) = −3.35 × 10−4 (GPa)−1.
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  • 8
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 384-387 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: NRCVAX is a complete system of programs, covering all aspects of crystal structure analysis from data reduction to the presentation of results. The system, which is written in a `neutral' Fortran 77, presently exists in two forms. The first runs on a VAX computer under VMS, on an 80386 PC under UNIX and under IBM VM/CMS and MVS/TSO. The second is an adaptation which runs on PC-XT, AT, PS/2 and comparable microcomputers under MS-DOS. The two versions differ somewhat in structure, but very little in code, operation or functionality except for the graphics. The many options of the programs can be selected in a highly interactive manner and because of this the system is very flexible. Most options are assigned default values, however, and it is usually safe to run the routines with a minimum of user input using the defaults. The system will accept data from a wide variety of sources and has interface routines for several other systems. Graphics in the VAX/UNIX version are based on the widely available Tektronix 4000 series protocol, while the microcomputer version supports most common display adapters. It is also possible to prepare files for a variety of plotters, dot-matrix printers and laser printers. Source code is distributed and it should not be difficult to adapt the system to any computer with virtual memory and a Fortran 77 compiler.
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  • 9
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 394-395 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 22 (1989), S. 396-397 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Type of Medium: Electronic Resource
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