Skip to main content
Log in

Separation of stereoisomers of tetramethylcalix[4]arenoctol and derivatives by high-performance liquid chromatography

  • Originals
  • Published:
Chromatographia Aims and scope Submit manuscript

Summary

A high performance liquid chromatographic procedure on 5 μm RP-18 was developed for the separation of the four possible cis-trans isomers of tetramethyl-calix[4]arenoctol, and of their octaacetates, and their octamethyl ethers.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. C. D. Gutsche, “Calixarenes” The Royal Society of Chemistry, Cambridge 1989, Vol. 1 of J. F. Stoddart (Ed.): “Monographs in Supramolecular Chemistry”.

  2. J. Vicens, V. Böhmer (Editors), “Calixarenes: A Versatile Class of Macrocyclic Compounds”, Kluwer Academic Publishers, Dordrecht, Boston, London, 1991.

    Google Scholar 

  3. D. J. Cram, S. Karbach, H.-E. Kim, C. B. Knobler, E. F. Maverick, J. L. Ericson, R. C. Helgesou, J. Am. Chem. Soc.110, 2229 (1988).

    Google Scholar 

  4. A. G. S. Högberg, J. Org. Chem.45, 4498 (1980).

    Google Scholar 

  5. A. G. S. Högberg, J. Am. Chem. Soc.102, 6046 (1980).

    Google Scholar 

  6. F. Weinelt, H.-J. Schneider, J. Org. Chem.56, 5527 (1991).

    Google Scholar 

  7. G. Mann, K. Müller, Workshop on Calixarenes and Related Compounds, Mainz, 1991.

  8. F. Weinelt, B. Noll, H. Weinelt, S. Hauptmann, G. Mann, D. Ehrhardt, C. Groth, W. Mertens, Ger. Pat. DD C 07 C/320 058 0 (23.09.88)

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Mann, G., Tittelbach-Helmrich, V., Lippmann, T. et al. Separation of stereoisomers of tetramethylcalix[4]arenoctol and derivatives by high-performance liquid chromatography. Chromatographia 34, 453–456 (1992). https://doi.org/10.1007/BF02290235

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02290235

Key Words

Navigation