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Preparation of a novel forpolymer as fluid loss additive for high temperature oil well cementing

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Abstract

A novel fluid loss additive (FLA) was synthesized using 2-acrylamido-2-methyl-propane sulphonic acid, acrylic acid, N,N-dimethyl acrylamide and N-vinyl-2-pyrrolidone by aqueous solution polymerization. TGA spectrum indicated that the decomposition temperature of FLA was higher than 330°C. The fluid loss testing showed that the FLA had an outstanding property of reducing fluid loss at 203°C in salt water cement slurry and the amount of fluid loss was controlled about 100 mL when FLA dosage was 1.0%. Cement slurry with 0.1–1.5% FLA kept stable thickening time. A better performance of FLA was found in fresh water cement slurry than in salt water cement slurry.

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Authors and Affiliations

  1. School of Chemistry and Chemical Engineering, Shanghai University of Engineering Sciences, Shanghai, 201620, China

    Qiang Xiao, Pinhua Rao, Wenfa Xiao, Xinxin Liu & Wenqi Zhang

Authors
  1. Qiang Xiao
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  2. Pinhua Rao
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  3. Wenfa Xiao
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  4. Xinxin Liu
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  5. Wenqi Zhang
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Correspondence to Pinhua Rao.

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The text was submitted by the authors in English.

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Xiao, Q., Rao, P., Xiao, W. et al. Preparation of a novel forpolymer as fluid loss additive for high temperature oil well cementing. Russ J Appl Chem 87, 1377–1381 (2014). https://doi.org/10.1134/S1070427214090328

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  • DOI: https://doi.org/10.1134/S1070427214090328

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