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Ultratrace Analysis of Dopamine Using a Combination of Imprinted Polymer-Brush-Coated SPME and Imprinted Polymer Sensor Techniques

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Abstract

A combination approach in solid-phase microextraction, based on a molecularly imprinted polymer-brush coating on an optical fiber coupled with a complementary molecularly imprinted polymer sensor, has been adopted for isolation, preconcentration, and analysis of dopamine at ultratrace levels in highly dilute aqueous samples. This combination enabled enhanced (up to 8.5-fold) preconcentration of the analyte, which is appropriate for achieving a stringent detection limit in clinical diagnosis of several neurodegenerative diseases. The detection limit of dopamine in biological samples was 0.018 ng mL−1 with a relative standard deviation less than 2.1% and without any non-specific contributions.

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Acknowledgement

Support of this work by the Department of Science and Technology, New Delhi, through project SR/S1/IC-18/2006, is gratefully acknowledged.

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Authors and Affiliations

  1. Analytical Division, Faculty of Science, Department of Chemistry, Banaras Hindu University, Varanasi, 221005, India

    Bhim Bali Prasad, Khushaboo Tiwari, Meenakshi Singh, Piyush S. Sharma, Amit K. Patel & Shrinkhala Srivastava

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  1. Bhim Bali Prasad
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  2. Khushaboo Tiwari
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  3. Meenakshi Singh
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  4. Piyush S. Sharma
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  5. Amit K. Patel
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  6. Shrinkhala Srivastava
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Correspondence to Bhim Bali Prasad.

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Prasad, B.B., Tiwari, K., Singh, M. et al. Ultratrace Analysis of Dopamine Using a Combination of Imprinted Polymer-Brush-Coated SPME and Imprinted Polymer Sensor Techniques. Chroma 69, 949–957 (2009). https://doi.org/10.1365/s10337-009-1039-6

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