Conclusions
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1.
The reaction of the trinitromethyl radical, generated electrochemically, with cyclic ethers leads to the formation of the correspondingα-trinitromethyl-substituted derivatives.
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2.
In the reaction products of the trinitromethyl radical with cyclic ethers were detected small amounts of theα-dinitromethyl derivatives of these ethers.
Literature cited
O. P. Shitov, S. L. Ioffe, V. A. Tartakovskii, and S. S. Novikov, Izv. Akad. Nauk SSSR, Ser. Khim., 490 (1972).
L. G. Feoktistov, S. A. Shevelev, V. A. Kokorekina, and A. A. Fainzil'berg, ibid., 1400 (1969).
S. A. Shevelev, V. A. Kokorekina, L. G. Feoktistov, and A. A. Fainzil'berg, Élektrokhimiya,6, 1244 (1970).
V. A. Kokorekina, S. A. Shevelev, L. G. Feoktistov, and A. A. Fainzil'berg, Izv. Akad. Nauk SSSR, Ser. Khim., 1717 (1972).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 11, pp. 2603–2604, November, 1972.
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Kokorekina, V.A., Shitov, O.P., Feoktistov, L.G. et al. Reaction of trinitromethyl radical with cyclic ethers. Russ Chem Bull 21, 2535–2536 (1972). https://doi.org/10.1007/BF00850115
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DOI: https://doi.org/10.1007/BF00850115