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High-performance ligand exchange chromatography on chiral diamine-bonded silica gel

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Summary

The resolution of racemates on chiral chemically bonded silica gel by high-performance ligand-exchange chromatography is described. The stationary phase was prepared by bonding (−) trans 1,2 cyclohexanediamine to silica gel through the coupling agent 3-glycidoxypropyl silane. The resolution of several α-amino acids and of compounds of pharmaceutical interest is reported.

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Authors and Affiliations

  1. Istituto di Cromatografia del CNR, Area della Ricerca di Roma, 00016, Monterotondo Stazione, C.P. 10, Italy

    C. Corradini, F. Federici & M. Sinibaldi

  2. Dipartimento di Chimica, Università degli Studi di Roma, “La Sapienza” P.Le Aldo Moro, 5, 00185, Roma, Italy

    A. Messina

Authors
  1. C. Corradini
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  2. F. Federici
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  3. M. Sinibaldi
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  4. A. Messina
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Corradini, C., Federici, F., Sinibaldi, M. et al. High-performance ligand exchange chromatography on chiral diamine-bonded silica gel. Chromatographia 23, 118–120 (1987). https://doi.org/10.1007/BF02312886

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  • DOI: https://doi.org/10.1007/BF02312886

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