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  • 1
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    Linking speleothem and soil magnetism in the Pau d'Alho cave (central South America) (2016)
    Wiley
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    Publication Date: 2016-09-20
    Description: Mineral magnetism of Pau d'Alho cave sediments, soils outside the cave and in the stalagmite #6 (ALHO6) in Midwest Brazil are presented. This high growth-rate speleothem (~168 mm/ka) encompasses the past 1355 years. Oxygen and carbon isotope data from the same stalagmite allow for a direct comparison of the magnetic signal with changes in paleoprecipitation and soil dynamics at the surface. Magnetic experiments include isothermal remanent magnetization (IRM), anhysteretic remanent magnetization (ARM), hysteresis loops, first order reversal curves (FORC), and low-temperature SQUID magnetometry. The main magnetic remanence carriers in ALHO6 are magnetite and goethite, with a nearly constant relative proportion. Remanent coercivities of magnetite in all our samples are within 14-17 mT for an average grain-size of ~1-2 µm, in the range of pedogenic magnetite, thus suggesting the detrital grains deposited in the stalagmite were produced in the soil above the cave. Magnetic remanence variations follow δ 13 C and δ 18 O data, suggesting a climatic control on the input of magnetic minerals into the Pau d'Alho cave system. The concentration of magnetic minerals in the stalagmite is governed by soil erosion above the cave, which by its turn is controlled by soil erosion and vegetation cover. Dry periods are associated with less stable soils and result in higher mineral fluxes carried into karst systems. Conversely, wetter periods are associated with soils topped by denser vegetation that retains micrometer-scale pedogenic minerals and thus reduces detrital fluxes into the cave.
    Print ISSN: 0148-0227
    Topics: Geosciences , Physics
    Published by Wiley on behalf of American Geophysical Union (AGU).
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  • 2
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    Domain wall pinning and dislocations: Investigating magnetite deformed under conditions analogous to nature using transmission electron microscopy (2015)
    Wiley
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    Publication Date: 2015-02-18
    Description: In this study, we deformed samples cut from a single magnetite octahedron and used transmission electron microscopy (TEM) and magnetic measurements to experimentally verify earlier computational models of magnetic domain wall pinning by dislocations and to better understand the nature of dislocations in magnetite. Dislocations in magnetite have been of interest for many decades because they are often cited as a likely source of stable thermoremanent magnetizations in larger multidomain (MD) magnetite grains, so a better understanding of dislocation effects on coercivity in MD magnetite is crucial. TEM imaging shows, for the first time, domain walls sweeping through the magnetite sample and being pinned at dislocations. In agreement with theory, these findings demonstrate that domain walls are more strongly pinned at networks of dislocations than at single dislocations and that domain walls pinned at longer dislocations have higher microcoercivities than those pinned at shorter dislocations. This experimentally illustrates the ability of dislocations to increase the coercivity of larger multidomain magnetite grains. The observed values for microcoercivity and bulk coercivity are in reasonable agreement with theoretical calculations. Burgers vectors were determined for some dislocations to verify that they were in keeping with expected dislocation orientations. The dislocations were found to be primarily located on close-packed 1 1 1 planes within the magnetite. Deformation caused only a minor change in bulk coercivity, but FORC diagrams show populations with increased coercivity not visible in hysteresis loops.
    Print ISSN: 0148-0227
    Topics: Geosciences , Physics
    Published by Wiley on behalf of American Geophysical Union (AGU).
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  • 3
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    Full vector low-temperature magnetic measurements of geologic materials (2015)
    Wiley
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    Publication Date: 2015-01-15
    Description: The magnetic properties of geologic materials offer insights into an enormous range of important geophysical phenomena ranging from inner core dynamics to paleoclimate. Often it is the low-temperature behavior (〈300K) of magnetic minerals that provides the most useful and highest sensitivity information for a given problem. Conventional measurements of low-temperature remanence are typically conducted on instruments that are limited to measuring one single axis component of the magnetization vector and are optimized for measurements in strong fields. These instrumental limitations have prevented fully optimized applications and have motivated the development of a low-temperature probe that can be used for low-temperature remanence measurements between 17 and 300K along three orthogonal axes using a standard 2G Enterprises SQuID rock magnetometer. In this contribution, we describe the design and implementation of this instrument and present data from five case studies that demonstrate the probe's considerable potential for future research: a polycrystalline hematite sample, a polycrystalline hematite and magnetite mixture, a single crystal of magnetite, a single crystal of pyrrhotite and samples of Umkondo Large Igneous Province diabase sills. This article is protected by copyright. All rights reserved.
    Electronic ISSN: 1525-2027
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Published by Wiley on behalf of American Geophysical Union (AGU).
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  • 4
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    The magnetism of mantle xenoliths and potential implications for sub-Moho magnetic sources (2013)
    Wiley
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    Publication Date: 2013-01-18
    Description: [1]  Mantle xenoliths provide our clearest look at the magnetic mineral assemblages below the Earth's crust. Previous investigations of mantle xenoliths suggested the absence of magnetite and metals, and proposed that even if such minerals were present, they would be above their Curie temperatures at mantle conditions. Here we use magnetic measurements to examine four exceptionally fresh suites of xenoliths, and show that magnetite occurs systematically, albeit in variable amounts depending on the tectonic setting. Specimens from low geotherm regions hold the largest magnetic remanence. Petrographic evidence shows that this magnetite did not form through serpentinization or other alteration processes. Magnetite, which is generally stable at the P-T- f O 2 conditions in the uppermost mantle, had to have formed either in the mantle or, less likely, in the volcanic conduit. In some cases, the source of the xenoliths was at temperatures 〈600°C, which may have allowed this portion of the lithospheric mantle to carry a magnetic remanence. Whether such magnetite carries a remanent magnetization or is simply the source of a strong induced magnetization, these new results suggest that the concept of the Moho as a major magnetic boundary needs to be revisited.
    Print ISSN: 0094-8276
    Electronic ISSN: 1944-8007
    Topics: Geosciences , Physics
    Published by Wiley on behalf of American Geophysical Union (AGU).
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  • 5
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    Phase Transformation and Particle-Mediated Growth in the Formation of Hematite from 2-Line Ferrihydrite (2016)
    American Chemical Society (ACS)
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    Publication Date: 2016-01-21
    Description: Crystal Growth & Design DOI: 10.1021/acs.cgd.5b01471
    Print ISSN: 1528-7483
    Electronic ISSN: 1528-7505
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Published by American Chemical Society (ACS)
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  • 6
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    Importance of titanohematite in detrital remanent magnetizations of strata spanning the Cretaceous-Paleogene boundary, Hell Creek region, Montana (2016)
    Wiley
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    Publication Date: 2016-02-06
    Description: Intermediate composition titanohematite, Fe 2-y Ti y O 3 with 0.5 ≤ y ≤ 0.7, is seldom the focus of paleomagnetic study and is commonly believed to be rare in nature. While largely overlooked in magnetostratigraphic studies, intermediate titanohematite has been identified as the dominant ferrimagnetic mineral in an array of Late Mesozoic and Early Cenozoic Laramide clastic deposits throughout the central United States. Intermediate titanohematite is ferrimagnetic and has similar magnetic properties to titanomagnetite, except its unique self-reversing property. Due to these similarities, and with detrital remanent magnetizations masking its self-reversing nature, intermediate titanohematite is often misidentified in sedimentary deposits. Past studies relied upon non-magnetic techniques including X-Ray diffraction and electron microprobe analysis. While these techniques can identify the presence of intermediate titanohematite, they fail to test whether the mineral is the primary recorder. To facilitate the identification of intermediate titanohematite in sedimentary deposits, we characterize this mineral using low-temperature magnetometry and high-temperature susceptibility experiments, and present a new identification technique based on titanohematite's self-reversing property, for sediments that span the Cretaceous-Paleogene boundary (Hell Creek region, Montana). Results from the self-reversal test indicate that the majority of remanence is held by minerals that become magnetized parallel to an applied field, but that intermediate, self-reversing titanohematite (y = 0.53–0.63) is an important ancillary carrier of remanence. While earlier literature suggests that intermediate titanohematite is rare in nature, reanalysis using specialized rock magnetic techniques may reveal that it's more abundant in the rock record, particularly within depositional basins adjacent to calc-alkaline volcanics, than previously thought. This article is protected by copyright. All rights reserved.
    Electronic ISSN: 1525-2027
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Published by Wiley on behalf of American Geophysical Union (AGU).
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  • 7
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    Low-temperature domain wall pinning in titanomagnetite: Quantitative modeling of multidomain first-order reversal curve diagrams and AC susceptibility (2011)
    Wiley
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    Publication Date: 2011-07-28
    Description: Domain wall pinning in titanomagnetite has been investigated at low temperatures using first-order reversal curve (FORC) diagrams, AC magnetic susceptibility, and Lorentz transmission electron microscopy. A discontinuous transition from a low-coercivity extrinsic pinning regime to a high-coercivity intrinsic pinning regime is evident in low-temperature FORC diagrams on cooling from 100 to 50 K. Intrinsic pinning is characterized by a “crescent moon” FORC distribution with narrow coercivity distribution centered on 10–20 mT. This crescent-shaped FORC distribution is reproduced using a modification of Néel's (1955) one-dimensional theory of domain wall pinning in a random field. The pinning transition coincides with a thermally activated relaxation process (activation energy 0.13 ± 0.01 eV), attributed to electron hopping. The relaxation and intrinsic pinning are explained as a magnetoelastic aftereffect caused by enhancement of magnetocrystalline anisotropy due to rearrangement and localization of Fe2+−Fe3+ cations within the domain walls. This study provides experimental verification that Néel's theory is an appropriate quantitative framework for the analysis of FORC diagrams in multidomain titanomagnetite and suggests a potential method for the quantitative unmixing of multidomain signals from FORC diagrams in rock and environmental magnetic studies.
    Electronic ISSN: 1525-2027
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Published by Wiley on behalf of American Geophysical Union (AGU).
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  • 8
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    Magnetic properties of ilmenite-hematite single crystals from the Ecstall pluton near Prince Rupert, British Columbia (2011)
    Wiley
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    Publication Date: 2011-09-10
    Description: Paleomagnetic studies of the 91 Ma Ecstall pluton and other Cretaceous plutons of British Columbia imply large northward tectonic movements (〉2000 km) may have occurred during the tectonic evolution of western North America. However, more recent studies have shown that the eastern edge of the Ecstall pluton experienced considerable mineralogical changes as younger Eocene plutons, such as the ∼58 Ma Quottoon Pluton, were emplaced along its margins. We investigated changes in the rock magnetic properties associated with this reheating event by examining isolated grains of intergrown ilmenite and hematite, the primary paleomagnetic recorder in the Ecstall pluton. Measurements of hysteresis properties, low-temperature remanence, and room temperature isothermal remanent magnetization acquisition and observations from magnetic force microscopy and off-axis electron holography indicate that samples fall into three groups. The groups are defined by the presence of mineral microstructures that are related to distance from the Quotoon plutonic complex. The two groups closest to the Quottoon Pluton contain magnetite within hematite and ilmenite lamellae. Reheating of the Ecstall pluton led to an increase in coercivity and magnetization, as well as to development of mixed phase hysteresis. These results indicate that shallow paleomagnetic directions from the western Ecstall pluton are not affected by reheating and are therefore likely to record original field conditions at the time of pluton emplacement. In the absence of structural deformation, these shallow inclinations are consistent with large-scale northward translation suggested by the Baja–British Columbia hypothesis.
    Electronic ISSN: 1525-2027
    Topics: Chemistry and Pharmacology , Geosciences , Physics
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  • 9
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    Rock magnetic properties of a soil developed on an alluvial deposit at Buttermilk Creek, Texas, USA (2011)
    Wiley
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    Publication Date: 2011-12-28
    Description: The evolution of magnetization within a floodplain soil begins with initial deposition of magnetic particles during sedimentation and continues via subsequent alteration and growth of iron-bearing compounds by pedogenic and biologic processes. Measurements of soil magnetic properties capture information about the developmental history of the soil and are a convenient method by which to investigate environmental change and pedogenesis. Using a range of magnetic measurements, a comprehensive scenario for soil development was constructed for floodplain sediments at the Debra L. Friedkin site, an important archeological site near Buttermilk Creek, Texas. Floodplain deposits have traditionally been avoided for soil magnetism studies because it is thought that the episodic input of sediment would form soils characterized by discrete sedimentary units rather than a continuous record of pedogenesis. We demonstrate that alluvial deposits can sometimes carry a straightforwardly interpretable magnetic signal similar to those typically seen in loess deposits. Smooth variation of rock magnetic parameters as a function of depth also leads us to conclude that the soil at this site is largely undisturbed and that the age of lithic artifacts found within the soil may be interpreted within stratigraphic context.
    Electronic ISSN: 1525-2027
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Published by Wiley on behalf of American Geophysical Union (AGU).
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  • 10
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    Mineral magnetism of dusty olivine: A credible recorder of pre-accretionary remanence (2011)
    Wiley
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    Publication Date: 2011-12-17
    Description: The magnetic properties of olivine-hosted Fe-Ni particles have been studied to assess the potential of “dusty olivine” to retain a pre-accretionary remanence in chondritic meteorites. Both body-centered (bcc) and face-centered cubic (fcc) Fe-Ni phases were formed by reduction of a terrestrial olivine precursor. The presence of Ni complicates the magnetic properties during heating and cooling due to the fcc-bcc martensitic transition. First-order reversal curve (FORC) diagrams contain a central ridge with a broad coercivity distribution extending to 600 mT, attributed to non-interacting single-domain (SD) particles, and a “butterfly” structure extending to 250 mT, attributed to single-vortex (SV) states. SD and SV states were imaged directly using electron holography. The location of the SD/SV boundary is broadly consistent with theoretical predictions. A method to measure the volume of individual SD particles using electron holography is presented. Combining the volume information with constraints on coercivity, we calculate the thermal relaxation characteristics of the particles and demonstrate that the high-coercivity component of remanance would remain stable for 4.6 Ga, even at temperatures approaching the Curie temperature of pure Fe. The high coercivity of the particles, together with the chemical protection offered by the surrounding olivine, is likely to make them resistant to shock remagnetization, isothermal remagnetization and terrestrial weathering, making dusty olivine a credible recorder of pre-accretionary magnetic fields.
    Electronic ISSN: 1525-2027
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Published by Wiley on behalf of American Geophysical Union (AGU).
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