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  • 1
    Electronic Resource
    Electronic Resource
    Modification of starch by graft copolymerisation with methyl methacrylatePresented at 12th National Conference of the Chemical Society of Nigeria, Calabar, Nigeria, Sept. 23-25, 1987. (1988)
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 163 (1988), S. 93-99 
    Details
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Methylmethacrylat (MMA) wurde mit Hilfe von Cerammoniumnitrat als Initiator auf Stärke gepfropft. Die Pfropfcopolymeren wurden durch selektive Lösungsextraktion in einem Soxhlet-Extraktor isoliert. Der Einfluß von Reaktionszeit, Initiatorkonzentration, Temperatur sowie der Monomer- und Särekonzentration auf die Pfropfausbeute wurde untersucht. Eine erste Studie der Kinetik dieser Pfropfcopolymerisationsreaktion zeigt, daß sie dem üblichen kinetischen Verhalten einer Radikalpolymerisation folgt.
    Notes: Methyl methacrylate (MMA) was grafted onto starch using ceric ammonium nitrate as initiator. The graft copolymers were isolated by selective solvent extraction in a Soxhlet apparatus. The effects of reaction time, initiator concentration, temperature, monomer, and acid concentrations on the graft yields were investigated. A preliminary kinetic study of the graft copolymerisation reactions shows that they follow the conventional kinetic behaviour of free radical polymerisation.
    Additional Material: 5 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/apmc.1988.051630108
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  • 2
    Electronic Resource
    Electronic Resource
    Adhesion studies of tyre cords with rubber. I. Synthesis and characterization of natural rubber graft copolymers (1992)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 44 (1992), S. 233-238 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Glycidyl methacrylate and N-vinyl pyrrolidone have been grafted onto natural rubber at 32°C using the simultaneous cobalt-60 irradiation technique. The natural rubber samples were swollen in the monomers for 24 h and thereafter subjected to gamma irradiation. The homopolymers formed in the graft copolymerization reactions and unreacted monomer were removed by solvent extraction using acetone and methanol for glycidyl methacrylate and N-vinyl pyrrolidone monomer, respectively. The influence of total dose and monomer concentration on the graft parameters was investigated. The dependence of the rate of grafting on the monomer concentration was found to be 0.93 and 0.80 for glycidyl methacrylate and N-vinyl pyrrolidone, respectively. DSC and TGA studies of the polymers were undertaken. Grafted copolymers based on glycidyl methacrylate were relatively less thermally stable compared with ungrafted natural rubber.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1992.070440206
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  • 3
    Electronic Resource
    Electronic Resource
    Graft polymerization of acrylamide onto cellulose acetate initiated by ceric ion (1991)
    Weinheim : Wiley-Blackwell
    Acta Polymerica 42 (1991), S. 279-281 
    Details
    ISSN: 0323-7648
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Unter Verwendung der Cerionenmethode wurde Acrylamid auf Celluloseacetat gepfropft. Der Einfluß verschiedener Reaktionsbedingungen auf den Pfropfgrad wurde untersucht. Die Aktivierungsenergie sowie die Reaktionsordnung bezüglich Monomer- und Initiatorkonzentration wurden bestimmt.
    Notes: The ceric ion method has been used to graft copolymerize acrylamide onto cellulose acetate. The effects of different reaction conditions on the graft yields were investigated. The activation energy and the order of reaction with respect to monomer and initiator concentration have been determined.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/actp.1991.010420610
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