ALBERT

Description: A superconducting linac will provide electron bunches of 17.5 GeV beam energy for the operation of the European X-ray Free Electron Laser (XFEL) at DESY. 800 superconducting niobium 1.3 GHz nine cell cavities and 100 superconducting magnet packages will be cooled in a liquid helium II cooling bath at 2.0K temperature. Liquid helium II bath cooling at 2.0K is established by means of a 4 stages cold compressor system. For the stable operation of cold compressors sudden load changes should be avoided. Electrical heaters in the helium II bath will compensate dynamic heat load changes caused by the radio frequency (RF) operation of the cavities in the XFEL linac. The complementary load operation of electrical heaters is studied at the existing facilities at DESY. Measurements performed at Cryo Module Test Bench (CMTB), Accelerator Module Test Facility (AMTF) and FLASH accelerator are reported.

Description: The European XFEL project is under construction at DESY in Germany. The superconducting XFEL linac is supplied by the XFEL helium refrigerator plant. This plant consists of two existing refrigerators, which were in service for the HERA storage ring until 2007. Since the XFEL linear accelerator requires cryogenic cooling at 2K, the existing cryogenic infrastructure had to be modified. Two of the three existing HERA helium refrigerators were required to cover the design heat load of the XFEL-linac. The refrigerator infrastructure was extended by a 2 K cooling loop, whose main component consists of a string of four cold compressors generating approximately 1.7 kW isothermal cooling capacity at 2K. The step by step commissioning and extension of the accelerator as well as the future upgrade option of the heat load demanded an extremely high turn down ability, a particular challenge for 2K cold compressor strings. The commissioning of the helium refrigerator infrastructure is underway...

Description: In order to produce pulsed electron beam with the energy of 17.5 GeV, the XFEL linear accelerator is under construction. After the assembly but before being installed in the accelerator tunnel, 100 accelerator modules have to be tested in Accelerator Module Test Facility (AMTF). Two vertical cryostats and three horizontal test benches are devoted to the testing of cavities and cryomodules as well as two other cold boxes and liquid helium (LHe) storage tank are installed to enable their operation. This paper describes our experience with cryogenic operation of AMTF after two years of operation.

Description: Medium and strong hydrogen bonds are common in biological systems. Here, they provide structural support and can act as proton transfer relays to drive electron and/or energy transfer. Infrared spectroscopy is a sensitive probe of molecular structure and hydrogen bond strength but strongly hydrogen-bonded structures often exhibit very broad and complex vibrational bands. As an example, strong hydrogen bonds between carboxylic acids and nitrogen-containing aromatic bases commonly display a 900 cm −1 broad feature with a remarkable double-hump structure. Although previous studies have assigned this feature to the OH, the exact origin of the shape and width of this unusual feature is not well understood. In this study, we present ab initio calculations of the contributions of the OH stretch and bend vibrational modes to the vibrational spectrum of strongly hydrogen-bonded heterodimers of carboxylic acids and nitrogen-containing aromatic bases, taking the 7-azaindole—acetic acid and pyridine—acetic acid dimers as examples. Our calculations take into account coupling between the OH stretch and bend modes as well as how both of these modes are affected by lower frequency dimer stretch modes, which modulate the distance between the monomers. Our calculations reproduce the broadness and the double-hump structure of the OH vibrational feature. Where the spectral broadness is primarily caused by the dimer stretch modes strongly modulating the frequency of the OH stretch mode, the double-hump structure results from a Fermi resonance between the out of the plane OH bend and the OH stretch modes.

Description: The European X-ray Free Electron Laser (XFEL) is in operation at DESY. The superconducting XFEL linac will produce pulsed electron beam at an energy of 17.5 GeV. The linac consists of 768 superconducting niobium 1.3 GHz nine cell cavities and 96 superconducting magnet packages assembled in 96 cryomodules. Each cryomodule is 12 m long and includes a 2 K helium II bath circuit for the cavities, and 5/8 and 40/80 K thermal radiation shields. Before being installed in the XFEL linac tunnel all cryomodules were tested in the Accelerator Module Test Facility (AMTF.) In this paper methods and results of static and dynamic heat load measurements of all XFEL cryomodules are reported. A comparison with first integral heat load measurements in the XFEL linac is given.

Description: The RF operation of the about 800 superconducting 1.3 GHz 9-cell cavities of the XFEL linac requires helium II bath cooling at 2 K, corresponding to a vapor pressure of 3100 Pa. After the first cool-down of the XFEL linac to 4 K in December, 27 th 2016 the operation of the 2 K cryogenic system was started in January, 2 nd 2017. The 2 K cryogenic system consist of a 4-stage set of cold compressors to compress helium vapor at a mass flow of up to 100 g/s from 2400 Pa to about 110 kPa and a full flow bypass with an arrangement of heat exchangers and control valves. This paper describes the XFEL refrigerating plant, especially the 2 K cryogenic system, the tuning of the cold compressor regulation to adapt to the XFEL linac static and dynamic heat loads and experience of about 6 months of operation.

Description: Beam commissioning of the European X-ray Free Electron Laser (European XFEL project) is ongoing. Commissioning the XFEL cryogenic system has started by cooling down the XFEL injector section in December 2015. The stationary operation was continued until August 2016. After intermediate warming up of the complete XFEL cryogenic system, the commissioning of remaining components including the 1.5 km long superconducting XFEL linear accelerator (linac) has commenced and was completed in beginning of December 2016. After conclusive pressure and leak tests, and flushing the cooldown started on 11 December 2016. Stable 4.5 K operation both for the linac and injector was established on 28 December. In this paper the XFEL cryogenic system is introduced and the first cooldown of the XFEL linac is reported. The cooldown sequences are described and the measured cooldown evolution is presented. Thermal losses of single circuits are given. Preliminary conclusions with the review of critical po...

Description: Medium and strong hydrogen bonds are well known to give rise to broad features in the vibrational spectrum often spanning several hundred wavenumbers. In some cases, these features can span over 1000 cm −1 and even contain multiple broad peaks. One class of strongly hydrogen-bonded dimers that includes many different phosphinic, phosphoric, sulfinic, and selenic acid homodimers exhibits a three-peaked structure over 1500 cm −1 broad. This unusual feature is often referred to as the Hadži ABC structure. The origin of this feature has been debated since its discovery in the 1950s. Only a couple of theoretical studies have attempted to interpret the origin of this feature; however, no previous study has been able to reproduce this feature from first principles. Here, we present the first ab initio calculation of the Hadži ABC structure. Using a reduced dimensionality calculation that includes four vibrational modes, we are able to reproduce the three-peak structure and much of the broadness of the feature. Our results indicate that Fermi resonances of the in-plane bend, out-of-plane bend, and combination of these bends play significant roles in explaining this feature. Much of the broadness of the feature and the ability of the OH stretch mode to couple with many overtone bending modes are captured by including an adiabatically separated dimer stretch mode in the model. This mode modulates the distance between the monomer units and accordingly the strength of the hydrogen-bonds causing the OH stretch frequency to shift from 2000 to 3000 cm −1 . Using this model, we were also able to reproduce the vibrational spectrum of the deuterated isotopologue which consists of a single 500 cm −1 broad feature. Whereas previous empirical studies have asserted that Fermi resonances contribute very little to this feature, our study indicates that while not appearing as a separate peak, a Fermi resonance of the in-plane bend contributes substantially to the feature.

Description: In order to produce short pulsed electron beam of 17.5 GeV energy, the XFEL linear accelerator is being built at DESY in Hamburg. Before being installed in the accelerator tunnel, 103 accelerator modules have to be tested in Accelerator Module Test Facility (AMTF). Cavities and cryomodules are tested at two vertical cryostats and three horizontal test benches. Two valve boxes and a liquid helium (LHe) storage tank are installed to enable cryogenic operation of AMTF. This paper describes our experience of three years cryogenic operation of AMTF. All 800 cavities and almost all cryomodules have been tested. The test results and lessons learned are also summarized

Description: The measurement of coolant flow is important operational parameter for reliable operation of cryogenic system with superconducting magnets or cavities as well as for the system diagnostics in case of non-steady-state operation, e.g. during cool-down/warm-up or other transients. Proper flowmeter is chosen according to the different parameters, e.g. turn-down, operating temperature range, leak-tightness, pressure losses, long-term stability, etc. For helium cryogenics, the Venturi tube or Orifice, as well as Coriolis flow meters are often applied. For the present time, the orifices are usually used due to their simplicity and low costs, however, low turn-down range, large pressure drop, restriction of flow area, susceptibility to thermoacoustic oscillations limit their useful operation range. Operational characteristics of Venturi tubes is substantially improved in comparison to orifices, however, relative high costs and susceptibility to thermoacoustic oscillations still limit th...