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  • 2000-2004  (5)
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  • 1
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    Polyimide Precursor Solid Residuum (2001)
    In:  CASI
    Details
    Publication Date: 2019-07-10
    Description: A polyimide precursor solid residuum is an admixture of an aromatic dianhydride or derivative thereof and an aromatic diamine or derivative thereof plus a complexing agent, which is complexed with the admixture by hydrogen bonding. The polyimide precursor solid residuum is effectively employed in the preparation of polyimide foam and the fabrication of polyimide foam structures.
    Keywords: Nonmetallic Materials
    Format: application/pdf
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    NASA TECHNICAL REPORTS
  • 2
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    Unknown
    Films, Preimpregnated Tapes and Composites Made from Polyimide "Salt-Like" Solutions (2001)
    In:  CASI
    Details
    Publication Date: 2019-07-10
    Description: High quality films, preimpregnated tape (prepegs), and composites have been fabricated from polyimide precursor 'saltlike' solutions. These salt-like solutions have a low viscosity (5,000 to 10,000 cp) and a high solids content (50-65% by weight) and can be coated onto reinforcing fiber to produce prepegs with excellent tack and drape at 12-15% residual solvent (approximately 4-6% water from thermal imidization reaction). The processing of these types of prepegs significantly overcomes solvent removal problems and allows excellent fiber wet out. In addition, the physical characteristics of the polyimide precursor salt-like solutions permits processing into high-performance materials through the use of standard prepregging and composite fabrication equipment. The resultant composites are of high quality.
    Keywords: Nonmetallic Materials
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    NASA TECHNICAL REPORTS
  • 3
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    Unknown
    Hollow Polyimide Microspheres (2001)
    In:  CASI
    Details
    Publication Date: 2019-07-10
    Description: A shaped article composed of an aromatic polyimide has a hollow, essentially spherical structure and a particle size of about 100 to about 1500 micrometers, a density of about 1 to about 6 pounds/cubic foot and a volume change of 1 to about 20% by a pressure treatment of 30 psi for 10 minutes at room temperature. A syntactic foam, made of a multiplicity of the shaped articles which are bonded together by a matrix resin to form an integral composite structure, has a density of about 3 to about 30 pounds/cubic feet and a compression strength of about 100 to about 1400 pounds/sq inch.
    Keywords: Nonmetallic Materials
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    NASA TECHNICAL REPORTS
  • 4
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    Unknown
    Aromatic Polyimide Foam (2000)
    In:  CASI
    Details
    Publication Date: 2019-07-10
    Description: A mechanically undensified aromatic polyimide foam is made from an aromatic polyimide precursor solid residuum and has the following combination of properties: a density according to ASTM D-3574A of about 0.5 pounds/cu.ft to about 20 pounds/cu.ft; a compression strength according to ASTM D-3574C of about 1.5 psi to about 1500 psi; and a limiting oxygen index according to ASTM D-2863 of about 35% oxygen to about 75% oxygen at atmospheric pressure. The aromatic polyimide foam has no appreciable solid inorganic contaminants which are residues of inorganic blowing agents. The aromatic polyimide which constitutes the aromatic polyimide foam has a glass transition temperature (Tg) by differential scanning calorimetry of about 235 C to about 400 C; and a thermal stability of 0 to about 1% weight loss at 204 C as determined by thermogravinietric analysis (TGA). The aromatic polyimide foam has utility as foam insulation and as structural foam, for example, for aeronautical, aerospace and maritime applications.
    Keywords: Nonmetallic Materials
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    NASA TECHNICAL REPORTS
  • 5
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    Hollow Polyimide Microspheres (2000)
    In:  CASI
    Details
    Publication Date: 2019-07-10
    Description: A shaped article composed of an aromatic polyimide has a hollow, essentially spherical structure and a particle size of about 100 to about 1500 microns a density of about 1 to about 6 pounds/cubic ft and a volume change of 1 to about 20 percent by a pressure treatment of 30 psi for 10 minutes at room temperature. A syntactic foam, made of a multiplicity of the shaped articles which are bonded together by a matrix resin to form an integral composite structure, has a density of about 3 to about 30 pounds/cubic ft and a compression strength 2 of about 100 to about 1400 pounds/sq in.
    Keywords: Nonmetallic Materials
    Format: text
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    NASA TECHNICAL REPORTS
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