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High resolution 1H NMR spectra of 2,2′-biquinoline (1982)

Drake, J. A. G. ; Jones, D. W.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 18 (1982), S. 42-44

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ISSN: 0030-4921

Keywords: Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: From analysis and refinement by the LAOCOON III program of the 220 MHz 1H spectrum of 2,2′-biquinoline, recorded as a saturated solution in carbon disulphide, most derived chemical shifts and coupling constants are close to corresponding values in quinoline. However, H-3 is at 1.5 ppm lower field in 2,2′-biquinoline than in quinoline and the ortho-coupling 3J(34) in the heterocyclic ring is 0.5 Hz larger in 2,2′-biquinoline than in quinoline; fairly free rotation about the 2,2′ bond is inferred.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1270180110

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